2,2'-二甲基氧化偶氮苯合成路线 （共 6 条）
反应条件
1: 49 percent / 68percent aq. HNO3 / 0.5 h / 50 - 60 °C 2: 1.) SnCl2, HCl, AcOH / 1.) 2 h, 2.) C6H6, reflux, 1 h View Scheme
参考文献
Urbanski, Jerzy; Wolak, Ireneusz
Polish Journal of Chemistry, 1984 , vol. 58, # 10-12 p. 1035 - 1045
反应条件
1: 49 percent / 68percent aq. HNO3 / 0.5 h / 50 - 60 °C 2: 1.) SnCl2, HCl, AcOH / 1.) 2 h, 2.) C6H6, reflux, 1 h View Scheme
参考文献
Polish Journal of Chemistry, , vol. 58, # 10-12 p. 1035 - 1045
反应条件
antimony(V) pentachloride 1.) CCl4, overnight; 2.) nitrobenzene, 199-200 deg C, 0.5 h; Yield given. Multistep reaction;
参考文献
Yamamoto, Jiro; Nishigaki, Yukihiro; Umezu, Masahiro; Matsuura, Teruo
Tetrahedron, 1980 , vol. 36, p. 3177 - 3180
反应条件
tetrachloromethane; chlorosulphuric acid
参考文献
Lukaschewitsch; Kurdjumowa
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 1963,1972
Chem.Abstr., 1949 , p. 3800
反应条件
potassium permanganate; water
参考文献
Lock
Chemische Berichte, 1930 , vol. 63, p. 855,865
Journal fuer Praktische Chemie (Leipzig), 1933 , vol. <2>138, p. 51,54
反应条件
hydrazine hydrate; aluminium in methanol
1.75 h; microwave irradiation;
参考文献
Nanjundaswamy; Pasha
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 4 p. 1086 - 1089
