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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
麝香酮
合成路线
（共 157 条）
1026920-90-0
→
反应条件
956-82-1
麝香酮
反应条件
1.1: Na; EtOH / benzene / 18 h / Heating 2.1: hydrobromic acid 3.1: Mg; I2 / diethyl ether / 28 h / Heating 3.2: 42 percent / aq. HCl / diethyl ether / 1 h / 45 - 50 °C View Scheme
参考文献
Guo, Yuan; Wu, Xin-Liang; Li, Jian-Li; Xu, Ruo-Qian; Shi, Zhen
Synthetic Communications, 2005 , vol. 35, # 19 p. 2489 - 2494
57395-52-5
→
反应条件
956-82-1
麝香酮
反应条件
1.1: sonication 2.1: PPA / microwave irradiation 3.1: Na; EtOH / benzene / 18 h / Heating 4.1: hydrobromic acid 5.1: Mg; I2 / diethyl ether / 28 h / Heating 5.2: 42 percent / aq. HCl / diethyl ether / 1 h / 45 - 50 °C View Scheme
参考文献
Guo, Yuan; Wu, Xin-Liang; Li, Jian-Li; Xu, Ruo-Qian; Shi, Zhen
Synthetic Communications, 2005 , vol. 35, # 19 p. 2489 - 2494
135056-56-3
→
反应条件
956-82-1
麝香酮
反应条件
1.1: PPA / microwave irradiation 2.1: Na; EtOH / benzene / 18 h / Heating 3.1: hydrobromic acid 4.1: Mg; I2 / diethyl ether / 28 h / Heating 4.2: 42 percent / aq. HCl / diethyl ether / 1 h / 45 - 50 °C View Scheme
参考文献
Guo, Yuan; Wu, Xin-Liang; Li, Jian-Li; Xu, Ruo-Qian; Shi, Zhen
Synthetic Communications, 2005 , vol. 35, # 19 p. 2489 - 2494
1732-10-1
壬二酸二甲酯
→
反应条件
956-82-1
麝香酮
反应条件
1: 85 percent / barium hydroxyde octahydrate / methanol / 4 d, - 10 deg C; 10 h, RT 2: 80 percent / 5percent KOH / methanol / 45 °C / electrolysis: anode: platinum foil; current source: galvanostat; current density 220 mA cm-2; current consumption: 1.4 F mol-1; cell voltage 20 V 3: 6 percent / potassium tert-butoxide / decahydronaphthalene / 48 h / 190 °C 4: 82 percent / diisopropylamine, n-butyllithium / tetrahydrofuran; hexane / 0 deg C, 30 min; -78 deg C, 1 h; RT, 1 h 5: 80 percent / Pd(OAc)2 / acetonitrile 6: 87 percent / copper(I) iodide / diethyl ether / Ambient temperature View Scheme
参考文献
Weiper-Idelmann, Andreas; Aus Dem Kahmen, Martin; Schaefer, Hans J.; Gockeln, Marianne
Acta Chemica Scandinavica, 1998 , vol. 52, # 6 p. 672 - 682
2104-19-0
壬二酸氢甲酯
→
反应条件
956-82-1
麝香酮
反应条件
1: 80 percent / 5percent KOH / methanol / 45 °C / electrolysis: anode: platinum foil; current source: galvanostat; current density 220 mA cm-2; current consumption: 1.4 F mol-1; cell voltage 20 V 2: 6 percent / potassium tert-butoxide / decahydronaphthalene / 48 h / 190 °C 3: 82 percent / diisopropylamine, n-butyllithium / tetrahydrofuran; hexane / 0 deg C, 30 min; -78 deg C, 1 h; RT, 1 h 4: 80 percent / Pd(OAc)2 / acetonitrile 5: 87 percent / copper(I) iodide / diethyl ether / Ambient temperature View Scheme
参考文献
Weiper-Idelmann, Andreas; Aus Dem Kahmen, Martin; Schaefer, Hans J.; Gockeln, Marianne
Acta Chemica Scandinavica, 1998 , vol. 52, # 6 p. 672 - 682
19102-90-0
十六碳二酸二甲酯
→
反应条件
956-82-1
麝香酮
反应条件
1: 6 percent / potassium tert-butoxide / decahydronaphthalene / 48 h / 190 °C 2: 82 percent / diisopropylamine, n-butyllithium / tetrahydrofuran; hexane / 0 deg C, 30 min; -78 deg C, 1 h; RT, 1 h 3: 80 percent / Pd(OAc)2 / acetonitrile 4: 87 percent / copper(I) iodide / diethyl ether / Ambient temperature View Scheme
参考文献
Weiper-Idelmann, Andreas; Aus Dem Kahmen, Martin; Schaefer, Hans J.; Gockeln, Marianne
Acta Chemica Scandinavica, 1998 , vol. 52, # 6 p. 672 - 682
101130-85-2
→
反应条件
956-82-1
麝香酮
反应条件
1: 1.) 322 deg C, 5 h, 2.) hydrolysis 2: 71 percent / H2 / Adams catalyst View Scheme
参考文献
Thies, Richard W.; Daruwala, Khushroo P.
Journal of the Chemical Society, Chemical Communications, 1985 , # 17 p. 1188 - 1189
101130-84-1
→
反应条件
956-82-1
麝香酮
反应条件
1: 1.) 318 deg C, 5 h, 2.) hydrolysis 2: 71 percent / H2 / Adams catalyst View Scheme
参考文献
Thies, Richard W.; Daruwala, Khushroo P.
Journal of the Chemical Society, Chemical Communications, 1985 , # 17 p. 1188 - 1189
1104-00-3
→
反应条件
956-82-1
麝香酮
反应条件
2: H2 / Pd-C View Scheme
参考文献
Nair,M.S.R. et al.
Journal of the Chemical Society, 1964 , p. 4154 - 4157
4277-06-9
→
反应条件
956-82-1
麝香酮
反应条件
2: Br2 4: (i) H2SO4, (ii) HN3 View Scheme
参考文献
Mookherjee,B.D. et al.
Journal of Organic Chemistry, 1971 , vol. 36, # 22 p. 3266 - 3270
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