2-(甲氧基羰基甲基)苯硼酸频那醇酯合成路线 （共 3 条）
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate in 1,4-dioxane
T=20°C; Inert atmosphereReflux;
参考文献
Yougnia, Rodrigue; Rochais, Christophe; Oliveira Santos, Jana Sopkova-de; Dallemagne, Patrick; Rault, Sylvain
Tetrahedron, 2010 , vol. 66, # 15 p. 2803 - 2808
反应条件
1: sulfuric acid / 20 - 65 °C / |Inert atmosphere
2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1-methyl-pyrrolidin-2-one / 39 h / 80 - 90 °C / |Inert atmosphere
View Scheme
参考文献
ELI LILLY AND COMPANY; HIPSKIND, Philip Arthur; STEPHENSON, Gregory Alan
Patent: US2013/29972 A1, 2013 ;
US 20130029972 A1
反应条件
1: dichloromethane / 20 °C / |Inert atmosphere
2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1-methyl-pyrrolidin-2-one / 39 h / 80 - 90 °C / |Inert atmosphere
View Scheme
参考文献
ELI LILLY AND COMPANY; HIPSKIND, Philip Arthur; STEPHENSON, Gregory Alan
Patent: US2013/29972 A1, 2013 ;
US 20130029972 A1
