反-8-甲基-6-壬酰氯合成路线 （共 17 条）
反应条件
1: 2M NaNO2, 5M aq. HNO3 / 0.5 h / 70 - 75 °C 2: thionyl chloride / 1.) room temp., 8 h, 2.) 100 deg C, 0.5 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 54, p. 3477 - 3478
反应条件
1: KOtBu / dimethylformamide / Ambient temperature 2: HNO3, NaNO2 / 1 h / 75 °C 3: 78 percent / CrO3 / acetone 4: SOCl2 / 2 h / Heating View Scheme
参考文献
Bioscience, Biotechnology, and Biochemistry, , vol. 56, # 6 p. 946 - 948
反应条件
1: HNO3, NaNO2 / 1 h / 75 °C 2: 78 percent / CrO3 / acetone 3: SOCl2 / 2 h / Heating View Scheme
参考文献
Bioscience, Biotechnology, and Biochemistry, , vol. 56, # 6 p. 946 - 948
反应条件
1: 78 percent / CrO3 / acetone 2: SOCl2 / 2 h / Heating View Scheme
参考文献
Bioscience, Biotechnology, and Biochemistry, , vol. 56, # 6 p. 946 - 948
反应条件
in diethyl ether 72 h; Ambient temperature;
参考文献
Kaga, Harumi; Goto, Kouhei; Fukuda, Takashi; Orito, Kazuhiko
Bioscience, Biotechnology, and Biochemistry, 1992 , vol. 56, # 6 p. 946 - 948
反应条件
1: pyridine / 18 h / Inert atmosphere 2: hydrogenchloride; water / ethanol / 18 h / 20 °C / Inert atmosphere View Scheme
参考文献
Barbero, Gerardo F.; Molinillo, Jose M. G.; Varela, Rosa M.; Palma, Miguel; MacIas, Francisco A.; Barroso, Carmelo G.
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 6 p. 3342 - 3349
反应条件
1: diethyl ether / 72 h / Ambient temperature 2: H2 / 10percent Pd/C / ethanol / 4 h / 760 Torr View Scheme
参考文献
Gannett, Peter M.; Nagel, Donald L.; Reilly, Pam J.; Lawson, Terence; Sharpe, Jody; Toth, Bela
Journal of Organic Chemistry, 1988 , vol. 53, # 5 p. 1064 - 1071
