2,2'-联吡啶-4,6'-二胺合成路线 （共 4 条）
反应条件
1.1: toluene-4-sulfonic acid / toluene / |Heating
2.1: tert.-butyl lithium / tetrahydrofuran / -78 °C
2.2: 20 °C
3.1: hydroxylamine hydrochloride; triethylamine / ethanol; water / |Heating
View Scheme
参考文献
Kremer, Christopher; Schnakenburg, Gregor; Lutzen, Arne
Beilstein Journal of Organic Chemistry, 2014 , vol. 10, p. 814 - 824
反应条件
1.1: toluene-4-sulfonic acid / toluene / |Heating
2.1: tert.-butyl lithium / tetrahydrofuran / -78 °C
2.2: 20 °C
3.1: hydroxylamine hydrochloride; triethylamine / ethanol; water / |Heating
View Scheme
参考文献
Kremer, Christopher; Schnakenburg, Gregor; Lutzen, Arne
Beilstein Journal of Organic Chemistry, 2014 , vol. 10, p. 814 - 824
反应条件
1.1: tert.-butyl lithium / tetrahydrofuran / -78 °C
1.2: 20 °C
2.1: hydroxylamine hydrochloride; triethylamine / ethanol; water / |Heating
View Scheme
参考文献
Kremer, Christopher; Schnakenburg, Gregor; Lutzen, Arne
Beilstein Journal of Organic Chemistry, 2014 , vol. 10, p. 814 - 824
反应条件
1.1: tert.-butyl lithium / tetrahydrofuran / -78 °C
1.2: 20 °C
2.1: hydroxylamine hydrochloride; triethylamine / ethanol; water / |Heating
View Scheme
参考文献
Kremer, Christopher; Schnakenburg, Gregor; Lutzen, Arne
Beilstein Journal of Organic Chemistry, 2014 , vol. 10, p. 814 - 824
