5-(二甲氧基甲基)-2-甲氧基吡啶合成路线 （共 6 条）
反应条件
hydrogenchloride in tetrahydrofuran 0.0833333 h;
参考文献
Bayer Aktiengesellschaft
Patent: US4990622 A1, 1991 ;
反应条件
1: 80 percent / tetrahydrofuran-d8 / 48 h / Ambient temperature; in a dry box
2: 60 percent / sodium / 4 h / Heating
View Scheme
参考文献
Dainter, Ronald S.; Jackson, Tracey; Omar, Abdirahman H. H.; Suschitzky, Hans; Wakefield, Basil J.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 283 - 287
反应条件
1: 64 percent / phosphorus pentachloride / 72 h / 115 °C
2: 80 percent / tetrahydrofuran-d8 / 48 h / Ambient temperature; in a dry box
3: 60 percent / sodium / 4 h / Heating
View Scheme
参考文献
Dainter, Ronald S.; Jackson, Tracey; Omar, Abdirahman H. H.; Suschitzky, Hans; Wakefield, Basil J.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 283 - 287
反应条件
in methanol
6 h; Heating;
参考文献
Dainter, Ronald S.; Jackson, Tracey; Omar, Abdirahman H. H.; Suschitzky, Hans; Wakefield, Basil J.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 283 - 287
反应条件
sodium
4 h; Heating;
参考文献
Dainter, Ronald S.; Jackson, Tracey; Omar, Abdirahman H. H.; Suschitzky, Hans; Wakefield, Basil J.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 283 - 287
参考文献
Dainter, Ronald S.; Suschitzky, Hans; Wakefield, Basil J.; Hughes, Nigel; Nelson, Anthony J.
Tetrahedron Letters, 1984 , vol. 25, # 49 p. 5693 - 5696
