1: With acetic acid in methanol
T=20°C; 0.166667 h;
2: With sodium cyanoborohydride; acetic acid in methanol
T=50°C; pH=5; 18 h;
3: With sodium hydrogencarbonate in methanol; water
参考文献
Wood, Michael R.; Gallicchio, Steven N.; Selnick, Harold G.; Zartman, C. Blair; Bell, Ian M.; Stump, Craig A.
Patent: US2007/265225 A1, 2007 ;
Location in patent: Page/Page column 53 ;
US 20070265225 A1
N-ethyl-N,N-diisopropylamine in acetonitrile
T=60°C; 6 h;
参考文献
Wood, Michael R.; Gallicchio, Steven N.; Selnick, Harold G.; Zartman, C. Blair; Bell, Ian M.; Stump, Craig A.
Patent: US2007/265225 A1, 2007 ;
Location in patent: Page/Page column 53 ;
US 20070265225 A1
