反应条件
1: 6.9 g / DIBAH / 1,2-dimethoxy-ethane; hexane / 2 h / 5 °C 2: 6.6 g / aq. CrO3, H2SO4 / acetone / 0.5 h / 5 °C 3: 2.7 g / CH2Cl2; diethyl ether / 0.17 h 4: 71.6 percent / aq. H2O2, (CCl3CO)2O / CH2Cl2 / 1.5 h / below 4 deg C View Scheme
参考文献
Grob; Boillaz; Schmidlin; Wehrli; Wieland; Fuhrer; Rihs; Joss; De Gasparo; Haenni; Ramjoue; Whitebread; Kalvoda
Helvetica Chimica Acta, 1997 , vol. 80, # 2 p. 566 - 585
