反应条件
1: sodium metaperiodate 2: 5percent H2SO4-AcOH / tetrahydrofuran / 3 h / Heating 4: 1.) H2, 5percent HCl, 2.) O3 / 1.) r.t., 4 d 5: 1.) O3, 2.) Me2S 6: sulphamic acid, sodium chlorite 7: H2SO4 / acetone 8: 52 percent / AlCl3, Me2S / CH2Cl2 / -10 °C 9: 68 percent / 5percent HCl / acetone / 24 h / 55 °C View Scheme
参考文献
Yamauchi, Masashige; Katayama, Sadamu; Todoroki, Toshiharu; Watanabe, Toshio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 389 - 394