反应条件
1: 29 percent / triphenylphosphine, iodine, pyridine / dioxane / 7 h / Ambient temperature 2: 78 percent / sodium methoxide / methanol / 16 h / Heating 3: iodine monochloride, sodium azide / dimethylformamide / 1 h / Ambient temperature 4: DAMP, pyridine 5: 1.) m-chloroperbenzoic acid, water, 2.) sodium methoxide / 1.) dichloromethane, RT, 3.5 h, 2.) methanol, RT, 30 min View Scheme
参考文献
Maag; Rydzewski; McRoberts; Crawford-Ruth; Verheyden; Prisbe
Journal of Medicinal Chemistry, 1992 , vol. 35, # 8 p. 1440 - 1451
