(3,4-二氯苯基)(2-吡啶基)甲酮合成路线 (共 3 条)
反应条件
pyridinium chlorochromate in dichloromethane
T=20°C; 0.333333 h;
参考文献
Froimowitz, Mark; Gu, Yonghong; Dakin, Les A.; Nagafuji, Pamela M.; Kelley, Charles J.; Parrish, Damon; Deschamps, Jeffrey R.; Janowsky, Aaron
Journal of Medicinal Chemistry, 2007 , vol. 50, # 2 p. 219 - 232
反应条件
1.1: Mg / iodine / tetrahydrofuran / 2 h / Heating
1.2: tetrahydrofuran / 2 h / 0 - 20 °C
2.1: pyridinium chlorochromate / CH2Cl2 / 0.33 h / 20 °C
View Scheme
参考文献
Froimowitz, Mark; Gu, Yonghong; Dakin, Les A.; Nagafuji, Pamela M.; Kelley, Charles J.; Parrish, Damon; Deschamps, Jeffrey R.; Janowsky, Aaron
Journal of Medicinal Chemistry, 2007 , vol. 50, # 2 p. 219 - 232
反应条件
1.1: Mg / iodine / tetrahydrofuran / 2 h / Heating
1.2: tetrahydrofuran / 2 h / 0 - 20 °C
2.1: pyridinium chlorochromate / CH2Cl2 / 0.33 h / 20 °C
View Scheme
参考文献
Froimowitz, Mark; Gu, Yonghong; Dakin, Les A.; Nagafuji, Pamela M.; Kelley, Charles J.; Parrish, Damon; Deschamps, Jeffrey R.; Janowsky, Aaron
Journal of Medicinal Chemistry, 2007 , vol. 50, # 2 p. 219 - 232