2,6-二溴-4-甲氧基苯胺合成路线 (共 2 条)
反应条件
n-butyllithium in diethyl ether; hexane T=-78°C; 1 h;
参考文献
Cossy; Poitevin; Pardo, D. Gomez; Peglion
Synthetic Communications, 1997 , vol. 27, # 20 p. 3525 - 3527
反应条件
sulfuric acid; hypophosphorous acid; sodium nitrite in toluene T=0°C; 4.5 h;
参考文献
Hartmann, Rolf; Frotscher, Martin; Oberwinkler, Sandrine; Ziegler, Erika; Messinger, Josef; Thole, Heinrich-Hubert
Patent: US2010/204234 A1, 2010 ;
Location in patent: Page/Page column 13 ;
US 20100204234 A1