dicobalt octacarbonyl in hexane
T=25°C; P=760 Torr; 20 h;
参考文献
Murai, Toshiaki; Yasui, Eiji; Kato, Shinzi; Hatayama, Yoshio; Suzuki, Satoshi; et al.
Journal of the American Chemical Society, 1989 , vol. 111, # 20 p. 7938 - 7946
1: With bis(cyclopentadienyl)titanium dichloride; zinc in tetrahydrofuran
0.5 h; Inert atmosphere;
2: With sodium dihydrogenphosphate; water in tetrahydrofuran
0.333333 h; Inert atmosphere;
1: 3-methyl-2-butenoic acid With cyclohexyl(iPr)NLi in tetrahydrofuran
T=0°C; 0.5 h;
2: (R)-phenylethylene oxide With lithium chloride in tetrahydrofuran
T=20°C; 16 h; Further stages.;
参考文献
Domingo, Luis R.; Gil, Salvador; Parra, Margarita; Segura, Jose
Molecules, 2008 , vol. 13, # 6 p. 1303 - 1311
1: 3-methyl-2-butenoic acid With cyclohexyl(iPr)NLi in tetrahydrofuran
T=0°C; 0.5 h;
2: (R)-phenylethylene oxide With lithium chloride in tetrahydrofuran
T=0°C; 16 h; Further stages.;
参考文献
Domingo, Luis R.; Gil, Salvador; Parra, Margarita; Segura, Jose
Molecules, 2008 , vol. 13, # 6 p. 1303 - 1311