(±)-2-氨基-1-丁醇合成路线 （共 59 条）
参考文献
Industrial and Engineering Chemistry, , vol. 32, p. 35
Journal of Organic Chemistry, , vol. 8, p. 11
参考文献
Annales de Chimie (Cachan, France), , vol. <8>26, p. 270
反应条件
in neat (no solvent) addn. of boron compd. to equimolar amt. of aminoalkanol, room temp.; driving out CH3NH2 in a stream of Ar, 20-25°C, 22h; distn. (vac.); elem. anal.; monocyclic: bicyclic isomer = 95:5;
参考文献
Chemische Berichte, , vol. 123, p. 2287 - 2302
反应条件
bis(bicyclo[2.2.1]hepta-2,5-diene)dichlorodirhodium; tributylphosphine; hydrogen in benzene T=120°C; Carbonylation; condensation; hydrogenation; P=60800 Torr; 6 h;
参考文献
Nagy, Emese; Heil, Balint; Toroes, Szilard
Journal of Organometallic Chemistry, 1999 , vol. 586, # 1 p. 101 - 105
参考文献
Rosen
Journal of the American Chemical Society, 1952 , vol. 74, p. 2994,2996
Full Text Show Details
Diamond Alkali Co.
Patent: US2860962 , 1954 ;
Full Text Show Details
Du Pont de Nemours and Co.
Patent: US2273424 , 1939 ;
参考文献
Havlicek, Libor; Hanus, Jan; Vesely, Jaroslav; Leclerc, Sophie; Meijer, Laurent; Shaw, Gordon; Strnad, Miroslav
Journal of Medicinal Chemistry, 1997 , vol. 40, # 4 p. 408 - 412
反应条件
potassium permanganate; sulfuric acid (+-)-2-amino-butyric acid;
参考文献
Billman; Parker; Smith
Journal of Biological Chemistry, 1949 , vol. 180, p. 30
反应条件
1: With (2R,3S)-(-)-di-O-benzoyl tartaric acid in acetone T=25°C; 6 h; 2: With potassium hydroxide in dichloromethane
参考文献
Periasamy, Mariappan; Sivakumar, Sangarappan; Reddy, Meda Narsi
Synthesis, 2003 , # 13 p. 1965 - 1967
反应条件
chiral stationary phase including isopropyl-functionalized CF6 in methanol; acetic acid; triethylamine; acetonitrile T=20°C; Purification / work up;
参考文献
Ingole, Pravin G.; Thakare, Neha R.; Kim, Keehong; Bajaj, Hari C.; Singh, Kripal; Lee, Hyungkeun
New Journal of Chemistry, 2013 , vol. 37, # 12 p. 4018 - 4024
反应条件
1: With (2R,3S)-(-)-di-O-benzoyl tartaric acid in acetone T=25°C; 6 h; 2: With potassium hydroxide in dichloromethane
参考文献
Periasamy, Mariappan; Sivakumar, Sangarappan; Reddy, Meda Narsi
Synthesis, 2003 , # 13 p. 1965 - 1967
