(±)-2-氨基-1-丁醇合成路线 (共 59 条)
反应条件
bis(bicyclo[2.2.1]hepta-2,5-diene)dichlorodirhodium; tributylphosphine; hydrogen in benzene T=120°C; Carbonylation; condensation; hydrogenation; P=60800 Torr; 6 h;
参考文献
Nagy, Emese; Heil, Balint; Toroes, Szilard
Journal of Organometallic Chemistry, 1999 , vol. 586, # 1 p. 101 - 105
反应条件
bis(bicyclo[2.2.1]hepta-2,5-diene)dichlorodirhodium; tributylphosphine; hydrogen in benzene T=120°C; Carbonylation; condensation; hydrogenation; P=60800 Torr; 6 h;
参考文献
Journal of Organometallic Chemistry, , vol. 586, # 1 p. 101 - 105
参考文献
Crank; Harding; Szinai
Journal of medicinal chemistry, 1970 , vol. 13, # 6 p. 1212 - 1215
反应条件
selenium; oxygen in acetonitrile T=30°C; P=760.051 Torr; 8 h;
参考文献
Li, Peng; Yuan, Xiaohua; Wang, Shudong; Lu, Shiwei
Tetrahedron, 2007 , vol. 63, # 50 p. 12419 - 12423
参考文献
Breslow,D.S. et al.
Journal of the American Chemical Society, 1967 , vol. 89, p. 2384 - 2390
反应条件
in dichloromethane 0.0833333 h; Ambient temperature;
参考文献
Kim, Sunggak; Ko, Young Kwan
Heterocycles, 1986 , vol. 24, # 6 p. 1625 - 1630
反应条件
nitromethane 0.0916667 h; Microwave irradiation;
参考文献
Bratulescu, George
Asian Journal of Chemistry, 2011 , vol. 23, # 2 p. 929 - 930
反应条件
methanol; sulfur T=120°C;
参考文献
Monsanto Chem. Co.
Patent: US2857393 , 1956 ;
反应条件
in toluene Ambient temperature;
参考文献
Maillard,J. et al.
Bulletin de la Societe Chimique de France, 1967 , p. 2110 - 2116
反应条件
selenium; oxygen in acetonitrile T=30°C; P=760.051 Torr; 8 h;
参考文献
Li, Peng; Yuan, Xiaohua; Wang, Shudong; Lu, Shiwei
Tetrahedron, 2007 , vol. 63, # 50 p. 12419 - 12423