1,3-二氯-2-丙醇合成路线 (共 217 条)
反应条件
hydrogenchloride; ε-caprolactone in water T=110°C; P=6448.83 Torr; 4 h; Product distribution / selectivity;
参考文献
WO2006/20234 A1, ;
Page/Page column 38-39 ;
反应条件
hydrogenchloride; acetic acid in water T=90°C; P=2052.96 Torr; 2 h; Product distribution / selectivity;
参考文献
WO2006/20234 A1, ;
Page/Page column 38 ;
反应条件
hydrogenchloride; malonic acid T=80 - 110°C; 3 h; Heating / reflux; Product distribution / selectivity;
参考文献
Siano, Dante; Santacesaria, Elio; Fiandra, Valeria; Tesser, Riccardo; Di Nuzzi, Giovanni; Di Serio, Martino; Nastasi, Mario
Patent: US2009/62574 A1, 2009 ;
Location in patent: Page/Page column 3 ;
反应条件
hydrogenchloride in dichloromethane 12 h; Ambient temperature;
参考文献
Kaupp, Gerd; Ulrich, Anke; Sauer, Gerhard
Journal fuer Praktische Chemie/Chemiker-Zeitung, 1992 , vol. 334, # 5 p. 383 - 390
反应条件
hydrogenchloride; acetic acid in water T=0 - 110°C; P=6448.83 Torr; 4 h; Product distribution / selectivity;
参考文献
WO2006/20234 A1, ;
Page/Page column 30-32 ;
反应条件
2,4,6-trichloro-1,3,5-triazine; 4-methylmorpholine N-oxide in chloroform T=-10 - 20°C;
参考文献
Rosenau, Thomas; Potthast, Antje; Kosma, Paul
Tetrahedron, 2002 , vol. 58, # 49 p. 9809 - 9815
反应条件
hydrogenchloride; 12-molybdophosphoric acid HPMo in water T=110°C; P=7500.75 Torr; 20 h; Homogenous liquid-phase; Product distribution / selectivity;
参考文献
WO2009/75402 A1, ;
Page/Page column 6-7; 8 ;
反应条件
in ethanol T=20°C; 36 h;
参考文献
WO2008/22062 A1, ;
Page/Page column 7-8 ;
反应条件
hydrogenchloride; polyacrylamide in water T=60 - 70°C; 60 - 80 h; Acidic aqueous solution; Product distribution / selectivity;
参考文献
WO2008/74733 A1, ;
Page/Page column 16-17 ;
反应条件
hydrogenchloride unter gleichzeitigem Abdestillieren des entstandenen Wassers;
参考文献
DE263106 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 11, p. 32