1: bromoacetic acid methyl ester With zinc in tetrahydrofuran 2: With Li-N,N-dimethyldithiocarbamat in tetrahydrofuran 3: bis(N,N-dimethyl thiocarbamoyl)-disulphide in tetrahydrofuran; dichloromethane T=20°C;
参考文献
Krasovskiy, Arkady; Gavryushin, Andrey; Knochel, Paul
Synlett, 2006 , # 5 p. 792 - 794
catalyst: hexamethylphosphoric triamide in benzene Ge-compd. addn. to degassed org. compd. soln., mercury liberation during 1.5 d; reaction mixt. fractionation; elem. anal.;
参考文献
Gendin, D. V.; Rybin, L. I.; Vyazankina, O. A.; Vyazankin, N. S.
Journal of General Chemistry USSR (English Translation), 1982 , vol. 52, p. 400 - 401
Zhurnal Obshchei Khimii, 1982 , vol. 52, p. 456 - 457