反应条件
1: 1) magnesium / 1) THF, -12 to -7 deg C, 1 h, 2) to room temperature, overnight
2: 68 percent / lithium aluminum hydride / diethyl ether / 0.5 h / 0 °C
3: 98 percent / triethylamine, DMAP / CH2Cl2 / 0 deg C to room temperature, overnight
View Scheme
参考文献
Coe, Diane M.; Parry, David M.; Roberts, Stanley M.; Storer, Richard
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 10 p. 2373 - 2378