反应条件
Multi-step reaction with 4 steps 1: 1) magnesium / 1) THF, -12 to -7 deg C, 1 h, 2) to room temperature, overnight2: 68 percent / lithium aluminum hydride / diethyl ether / 0.5 h / 0 °C3: 98 percent / triethylamine, DMAP / CH2Cl2 / 0 deg C to room temperature, overnight4: 1) dibromodimethylhydantoin, 2) potassium carbonate / 1) acetone, water, 0 deg C, 2) methanol, room temperature, overnight
参考文献
Coe, Diane M.; Parry, David M.; Roberts, Stanley M.; Storer, Richard Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 10 p. 2373 - 2378
