暂无反应条件数据

(i) BaCO3, H2O, (ii) aq. HCl; Multistep reaction;

1: sodium hydroxide / water / 1 h / 20 °C 2: chlorosulfonic acid / 4 h / 5 - 130 °C 3: ammonia / water / 10 - 20 °C 4: palladium 10 on activated carbon; hydrogen / methanol / 4 h / 50 °C View Scheme

1.1: N,N-dimethyl-formamide; thionyl chloride / 4 h / Reflux 2.1: ammonium hydroxide / toluene; water; tetrahydrofuran / 2 h / -10 °C / Reflux 2.2: pH 4 3.1: ammonium hydroxide; (NH4)2CO3; copper(II) sulfate / water / 72 h / 118 °C / Autoclave; Industry scale 4.1: hydrogen / 5 palladium on charcoal / ethanol; water / 8 h / 55 °C / Industry scale 5.1: pyridine / dichloromethane / 0 - 23 °C / Industry scale 6.1: tetrahydrofuran / 1 h / 0 - 23 °C / Industry scale 7.1: sodium hydroxide; water / 30 h / 23 °C / Industry scale 7.2: 0 °C / Industry scale View Scheme

1: 75 percent / LiOH*H2O / dimethylsulfoxide / 0.5 h / 110 °C 2: 95 percent / H2 / Pd-C / methanol; H2O / 2.5 h / 20 °C View Scheme

暂无反应条件数据

暂无反应条件数据

1.1: N,N-dimethyl-formamide; thionyl chloride / 4 h / Reflux 2.1: ammonium hydroxide / toluene; water; tetrahydrofuran / 2 h / -10 °C / Reflux 2.2: pH 4 3.1: ammonium hydroxide; (NH4)2CO3; copper(II) sulfate / water / 72 h / 118 °C / Autoclave; Industry scale View Scheme

in alkal. Loesung;

sodium hydroxide