4-甲氧基-2-硝基苯胺合成路线 （共 138 条）
反应条件
1: 96 percent / Na2S*9H2O / H2O / 6 h / Heating 2: 40 percent / potassium hydroxide / ethanol; H2O / 6 h / Heating View Scheme
参考文献
Mahajan; Nandre
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 7 p. 1756 - 1758
反应条件
tin(ll) chloride T=130°C; 0.0833333 h; microwave;
参考文献
Tetrahedron Letters, , vol. 46, # 39 p. 6741 - 6743
反应条件
1: nickel (II)-chloride; water 2: acetic acid; aqueous sulfuric acid 3: palladium; aqueous ammonia / 33097.9 Torr / Hydrogenation View Scheme
参考文献
Stephen et al.
Journal of the Chemical Society, 1947 , p. 1034,1037
反应条件
1: conc. aq. HCl, NaNO2 / H2O / 0.25 h / -5 - 2 °C 2: LiCl, CuCl*2H2O / H2O; acetone / 1.) 2 h, 3 to 10 deg C, 2.) 2 h, 10 deg C to room temp., 3.) 2 h, room temp. 3: Fe, HOAc, sodium acetate dihydrate / ethanol; H2O / 2 h / Heating View Scheme
参考文献
Raucher, Stanley; Koolpe, Gary A.
Journal of Organic Chemistry, 1983 , vol. 48, # 12 p. 2066 - 2069
反应条件
bei der Entamidierung;
参考文献
Reverdin
Bulletin de la Societe Chimique de France, 1897 , vol. <3> 17, p. 115
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Reverdin
Chemische Berichte, 1896 , vol. 29, p. 2598
Chemische Berichte, 1899 , vol. 32, p. 161 Anm.
反应条件
1: H2 / Raney Ni / ethanol / 1 h / 760 Torr / Ambient temperature 2: 82 percent / aq. SeO2 / ethanol 3: 87 percent / conc. H2SO4, fuming HNO3 / 1 h / Ambient temperature 4: 76 percent / conc. aq. HCl, conc. aq. HI / 2 h / Ambient temperature View Scheme
参考文献
Grivas, Spiros; Tian, Wei
Acta Chemica Scandinavica, 1992 , vol. 46, # 11 p. 1109 - 1113
反应条件
1.1: HBr / H2O; dioxane / 0.67 h / Heating 1.2: sodium nitrite / dioxane; H2O / 1 h / 0 °C 1.3: 85 percent / copper(I) bromide; HBr / dioxane; H2O / 0 - 60 °C 2.1: iron / ethanol; acetic acid / 2.5 h / Heating View Scheme
参考文献
Tidwell, Jeffrey H.; Buchwald, Stephen L.
Journal of Organic Chemistry, 1992 , vol. 57, # 24 p. 6380 - 6382
反应条件
1: (i) (oxidation), (ii) Cu, aq. HCl, EtOH 2: (i) NaNO2, H2SO4, AcOH, (ii) CuBr 3: Fe / aq. acetic acid View Scheme
参考文献
Kelley,W.S. et al.
Justus Liebigs Annalen der Chemie, 1971 , vol. 744, p. 129 - 141
反应条件
1: (i) NaNO2, H2SO4, AcOH, (ii) /BRN= 3594799/ 2: Py / acetic acid View Scheme
参考文献
Passerini,R.; Purrello,G.
Gazzetta Chimica Italiana, 1960 , vol. 90, p. 1277 - 1289
反应条件
1: 88 percent / CuBr2, t-BuONO / acetonitrile 2: Fe, HCl / ethanol 3: NaHCO3 / dimethylformamide 4: 1) t-BuLi, Cp2Zr(CH3)Cl, 2) I2 / 1) THF, -78 to 45 deg C, 2) CH2Cl2, 0 deg C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 57, # 24 p. 6380 - 6382
