反应条件
anhydrous lithium acetate; copper diacetate; methyl vinyl ketone; palladium diacetate in N,N-dimethyl-formamide byproducts: 4-phenyl-3-buten-2-one; under Ar; 0.30-0.36 mmol of organotin comp. and 0.30 mmol of olefin added to a soln. of 0.03 mmol of Pd(OAc)2, 0.90 mmol of Cu(OAc)2 and 0.60 mmol of LiOAc in DMF at room temp., mixt. stirred at 100° for 24 h, diluted with Et2O; monitored by NMR spectra;
参考文献
Hirabayashi, Kazunori; Ando, Jun-Ichi; Kawashima, Jun; Nishihara, Yasushi; Mori, Atsunori; Hiyama, Tamejiro
Bulletin of the Chemical Society of Japan, 2000 , vol. 73, # 6 p. 1409 - 1417
