azobis(isobutyronitrile) in neat (no solvent) High Pressure; (Ar); addn. of AIBN to stannane, addn. of GeCl4, heating to 150°Cfor 22 h in a sealed tube, cooling to room temp.; dissolving in CH2Cl2, vac. distn.;
PCy(1-pyrrolidinyl)2; 3 A molecular sieve; tetramethyl-ammonium fluoride; bis(η3-allyl-μ-chloropalladium(II)) in various solvent(s) T=20°C; Stille reaction;
参考文献
Angewandte Chemie - International Edition, , vol. 42, # 41 p. 5079 - 5082
