反应条件
1: 72.4 percent / N-iodosuccinimide, NaHCO3, tetrabutylammonium hydroxide / CH2Cl2; H2O / 0.5 h 2: 0.43 g / iodine / CH2Cl2 / 90 h / Ambient temperature; in the dark 3: PdCl2(Ph3P)2, CuI, Et3N 4: 31 percent / AgNO3, KCN / ethanol; H2O / 0.5 h / 0 °C / in the dark View Scheme
参考文献
Spencer, Robin W.; Tam, Tim Fat; Thomas, Everton; Robinson, Valerie J.; Krantz, Allen
Journal of the American Chemical Society, 1986 , vol. 108, # 18 p. 5589 - 5597
