4,7-二溴-2-辛基-2H-苯并三唑合成路线 （共 3 条）
反应条件
1: sodium hydride / dichloromethane; mineral oil / 72 h / 20 °C / |Inert atmosphere
2: bromine; hydrogen bromide / 48 h / 125 °C
View Scheme
参考文献
NITTO DENKO CORPORATION; RACHWAL, STANISLAW; WANG, PENG; RACHWAL, BOGUMILA; ZHANG, HONGXI; YAMAMOTO, MICHIHARU
Patent: US2013/74927 A1, 2013 ;
反应条件
1: sodium hydride / dichloromethane; mineral oil / 72 h / 20 °C / |Inert atmosphere
2: bromine; hydrogen bromide / 48 h / 125 °C
View Scheme
参考文献
NITTO DENKO CORPORATION; RACHWAL, STANISLAW; WANG, PENG; RACHWAL, BOGUMILA; ZHANG, HONGXI; YAMAMOTO, MICHIHARU
Patent: US2013/74927 A1, 2013 ;
反应条件
1: sodium hydroxide
2: bromine; hydrogen bromide
View Scheme
参考文献
Mao, Xuerong; Jiang, Xiaoxiang; Hu, Hongwen; Cheng, Yixiang; Zhu, Chengjian
Synlett, 2013 , vol. 24, # 12 art. no. ST-2013-W0300-L, p. 1505 - 1508
