2,4,6-三叔丁基苯胺合成路线 （共 27 条）
反应条件
methanol; sodium amalgam 12 h; Heating;
参考文献
Underiner, Gail E.; Tan, Robin P.; Powell, Douglas R.; West, Robert
Journal of the American Chemical Society, 1991 , vol. 113, # 22 p. 8437 - 8443
反应条件
1: 67 percent / HNO3 / acetic anhydride; acetic acid / 50 h / Ambient temperature 2: 56 percent / 5percent sodium amalgam / methanol / 5 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 104, # 25 p. 7191 - 7195
反应条件
base; 2-(α-hydroxyethyl)-3,4-dimethylthiazolium triflate in dichloromethane T=20°C;
参考文献
Ferreira, Luisa M.; Marques, M. Manuel B.; Gloria, Paulo M.C.; Chaves, Humberto T.; Franco, Joao-Pedro P.; Mourato, Isabel; Antunes, Jose-Rafael T.; Rzepa, Henry S.; Lobo, Ana M.; Prabhakar, Sundaresan
Tetrahedron, 2008 , vol. 64, # 33 p. 7759 - 7770
反应条件
1: 1.) AlCl3, 2.) AlCl3 / 1.) room temperature, 19 h 2: 67 percent / HNO3 / acetic anhydride; acetic acid / 50 h / Ambient temperature 3: 56 percent / 5percent sodium amalgam / methanol / 5 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 104, # 25 p. 7191 - 7195
反应条件
oxygen; triphenylphosphine in diethyl ether T=-78 - 0°C; 7 h; Yield given. Yields of byproduct given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 53, # 1 p. 205 - 209
反应条件
1: aluminium chloride / -3 °C 2: acetic acid; acetic acid anhydride; concentrated nitric acid 3: sodium-amalgam; methanol View Scheme
参考文献
Journal of the American Chemical Society, , vol. 76, p. 2349,2351
反应条件
in diethyl ether T=-78 - 20°C; 6.5 h; Yields of byproduct given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 53, # 1 p. 205 - 209
反应条件
in toluene T=-80 - -25°C; 2 h; or in ethyl acetate; Product distributionMechanism;
参考文献
Journal of Organometallic Chemistry, , vol. 312, p. 297 - 304
反应条件
hydrogen bromide; copper(I) bromide; sodium nitrite
参考文献
Betts; Barclay
Canadian Journal of Chemistry, 1955 , vol. 33, p. 1768,1769
反应条件
tert.-butylhydroperoxide; cobalt(II)salen in water; 1,2-dichloro-ethane T=23 - 24°C; 2.66667 h;
参考文献
Nishinaga; Forster; Eichhorn; Speiser; Rieker
Tetrahedron Letters, 1992 , vol. 33, # 31 p. 4425 - 4428
