反应条件
1: 99 percent / H2 / Lindlar / tetrahydrofuran / 0.75 h / 23 °C
2: 99 percent / potassium bromide / tetrahydrofuran; aq. acetic acid / 10 h / 0 °C
3: 92 percent / Jones reagens / 1.5 h / 23 °C
4: CHCl3 / 3 h / Heating
5: 1.) 1N aq.NaOH / 1.) chloroform, 23 grad C, 3 min; 2). benzene, 23 grad C, 10 h.
6: NaBH4 / methanol / 0.17 h / -40 °C
View Scheme
参考文献
Corey, E. J.; Su, Wei-guo
Tetrahedron Letters, 1984 , vol. 25, # 45 p. 5119 - 5122
