1: 1,2-bis(phosphino)benzene With sodium in tetrahydrofuran
48 h;
2: methyl iodide in tetrahydrofuran
T=-78 - 20°C; Further stages. Title compound not separated from byproducts.;
参考文献
Chatterjee; George; Salem; Willis
Journal of the Chemical Society, Dalton Transactions, 2001 , # 12 p. 1890 - 1896
1: 1,2-bis(phosphino)benzene With n-butyllithium in tetrahydrofuran
Metallation;
2: methyl iodide in tetrahydrofuran
Methylation; Further stages.;
参考文献
Chatterjee, Swarup; Doyle, Roy; Hockless, David C. R.; Salem, Geoffrey; Willis, Anthony C.
Journal of the Chemical Society, Dalton Transactions, 2000 , # 12 p. 1829 - 1830
1: 1,2-phenylenebis(methylphosphine) With potassium in ammonia
Metallation;
2: methyl iodide in tetrahydrofuran
Methylation; Title compound not separated from byproducts;
参考文献
Chatterjee, Swarup; Doyle, Roy; Hockless, David C. R.; Salem, Geoffrey; Willis, Anthony C.
Journal of the Chemical Society, Dalton Transactions, 2000 , # 12 p. 1829 - 1830
Chatterjee, Swarup; Doyle, Roy; Hockless, David C. R.; Salem, Geoffrey; Willis, Anthony C.
Journal of the Chemical Society, Dalton Transactions, 2000 , # 12 p. 1829 - 1830
Chatterjee, Swarup; Doyle, Roy; Hockless, David C. R.; Salem, Geoffrey; Willis, Anthony C.
Journal of the Chemical Society, Dalton Transactions, 2000 , # 12 p. 1829 - 1830
