(s)-(O-(N-苄基脯氨基酸)氨基I(苯基)..N,N,N-镍合成路线 (共 3 条)
反应条件
in tetrahydrofuran -70°C;;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 19 p. 1336 - 1338
反应条件
in tetrahydrofuran -70°C;;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 19 p. 1336 - 1338
反应条件
sodium methoxide in methanol a soln. of glycine in MeONa-MeOH was added to a soln. of the substituted benzophenone and Ni(NO3)2*6H2O in MeOH, mixt. was stirred for 2 h at 50°C under Ar, reaction was monitored by TLC; water was added, mixt. extd. with CHCl3, ext. evapd., residue purified on SiO2 and Sephadex LH-20 columns (eluents CHCl3-acetone and benzene-EtOH resp.); elem. anal.;
参考文献
Belokon, Yuri N.; Bulychev, Alexander G.; Vitt, Sergei V.; Struchkov, Yuri T.; Batsanov, Andrei S.; et al.
Journal of the American Chemical Society, 1985 , vol. 107, # 14 p. 4252 - 4259