反-1,2-双(苯基磺酰基)乙烯合成路线 （共 19 条）
反应条件
in N,N-dimethyl-formamide 3 h; Ambient temperature;
参考文献
Sepiol, Janusz; Soulen, Robert L.; Sepiol, Jadwiga
Journal of Fluorine Chemistry, 1983 , vol. 23, p. 163 - 170
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 10, p. 1059 - 1062
Zhurnal Organicheskoi Khimii, , vol. 10, # 5 p. 1050 - 1053
反应条件
1: aqueous hydrogen peroxide; acetic acid; sulfuric acid 2: methanol; sodium hydrogencarbonate View Scheme
参考文献
Gazzetta Chimica Italiana, , vol. 86, p. 428,431, 755
反应条件
methanol; sodium hydrogencarbonate
参考文献
Gazzetta Chimica Italiana, , vol. 86, p. 428,431, 755
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 53, # 27 p. 9269 - 9278
反应条件
sodium hydride 1.) THF, 0 deg C, 20 min, 2.) THF, 0 deg C, 3 h; Multistep reaction;
参考文献
Cossu, Sergio; De Lucchi, Ottorino; Fabris, Fabrizio; Ballini, Roberto; Bosica, Giovanna
Synthesis, 1996 , # 12 p. 1481 - 1484
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Benati, Luisa; Calestani, Gianluca; Nanni, Daniele; Spagnolo, Piero; Volta, Marco
Tetrahedron, 1997 , vol. 53, # 27 p. 9269 - 9278
反应条件
1: With triethylamine; triphenylphosphine; [Cu(I)(CH3CN)4]PF6 in tetrahydrofuran
T=20°C; 5 h;
2: With 1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran
T=20°C; 0.5 h; Further stages.;
参考文献
Lopez-Perez, Ana; Robles-Machin, Rocio; Adrio, Javier; Carretero, Juan Carlos
Angewandte Chemie - International Edition, 2007 , vol. 46, # 48 p. 9261 - 9264
反应条件
1: With triethylamine; triphenylphosphine; [Cu(I)(CH3CN)4]PF6 in tetrahydrofuran
T=20°C; 5 h;
2: With 1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran
T=20°C; 0.5 h; Further stages.;
参考文献
Lopez-Perez, Ana; Robles-Machin, Rocio; Adrio, Javier; Carretero, Juan Carlos
Angewandte Chemie - International Edition, 2007 , vol. 46, # 48 p. 9261 - 9264
