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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
96306-54-6
合成路线
（共 9 条）
96306-54-6
→
反应条件
125628-96-8
反应条件
1: ammonium formate / 10percent Pd/C / methanol / 0.5 h / Heating 2: 71 percent / 70percent HNO3; AcOH / 0.5 h / 20 °C 3: AlCl3; pyridine / ethyl acetate / 2 h / Heating View Scheme
参考文献
Learmonth, David A.; Vieira-Coelho, Maria A.; Benes, Jan; Alves, Paula C.; Borges, Nuno; Freitas, Ana P.; Soares-da-Silva, Patricio
Journal of Medicinal Chemistry, 2002 , vol. 45, # 3 p. 685 - 695
96306-72-8
→
反应条件
96306-54-6
反应条件
jones reagent in acetone 25 h; Ambient temperature;
参考文献
Tilley, Jefferson W.; Clader, John W.; Wirkus, Maria; Blount, John F.
Journal of Organic Chemistry, 1985 , vol. 50, # 13 p. 2220 - 2224
2426-87-1
4-苄氧基-3-甲氧基苯甲醛
→
反应条件
96306-54-6
反应条件
1: diethyl ether; tetrahydrofuran / 1 h / 20 °C 2: NaO-tBu; cyclohexanone / toluene / 0.5 h / Heating View Scheme
参考文献
Learmonth, David A.; Vieira-Coelho, Maria A.; Benes, Jan; Alves, Paula C.; Borges, Nuno; Freitas, Ana P.; Soares-da-Silva, Patricio
Journal of Medicinal Chemistry, 2002 , vol. 45, # 3 p. 685 - 695
100-39-0
溴化苄
→
反应条件
96306-54-6
反应条件
1: 93 percent / K2CO3 / acetone / 2 h / Heating 2: diethyl ether; tetrahydrofuran / 1 h / 20 °C 3: NaO-tBu; cyclohexanone / toluene / 0.5 h / Heating View Scheme
参考文献
Learmonth, David A.; Vieira-Coelho, Maria A.; Benes, Jan; Alves, Paula C.; Borges, Nuno; Freitas, Ana P.; Soares-da-Silva, Patricio
Journal of Medicinal Chemistry, 2002 , vol. 45, # 3 p. 685 - 695
121-33-5
香草醛
→
反应条件
96306-54-6
反应条件
1: 93 percent / K2CO3 / acetone / 2 h / Heating 2: diethyl ether; tetrahydrofuran / 1 h / 20 °C 3: NaO-tBu; cyclohexanone / toluene / 0.5 h / Heating View Scheme
参考文献
Learmonth, David A.; Vieira-Coelho, Maria A.; Benes, Jan; Alves, Paula C.; Borges, Nuno; Freitas, Ana P.; Soares-da-Silva, Patricio
Journal of Medicinal Chemistry, 2002 , vol. 45, # 3 p. 685 - 695
108-86-1
溴代苯
→
反应条件
96306-54-6
反应条件
1: 1.) Mg / 1.) THF, 2.) 15 min 2: 56 percent / 8N Jones reagent / acetone / 25 h / Ambient temperature View Scheme
参考文献
Tilley, Jefferson W.; Clader, John W.; Wirkus, Maria; Blount, John F.
Journal of Organic Chemistry, 1985 , vol. 50, # 13 p. 2220 - 2224
1027201-30-4
→
反应条件
96306-54-6
反应条件
hydrogenchloride in tetrahydrofuran; methanol; benzene 7 h; Heating; Yield given;
参考文献
Taniguchi, Kiyoshi; Miyao, Yasuhiro; Yamano, Katsuhiro; Yamamoto, Takao; Terai, Takao; Kusunoki, Takahiro; Tsubaki, Kazunori; Shiokawa, Youichi
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 6 p. 1188 - 1195
52805-34-2
4-苄氧基-3-甲氧基苯甲腈
→
反应条件
96306-54-6
反应条件
1: benzene / 1.) RT, 50 min, 2.) 70 deg C, 7 h 2: conc. aq. HCl / benzene; methanol; tetrahydrofuran / 7 h / Heating View Scheme
参考文献
Taniguchi, Kiyoshi; Miyao, Yasuhiro; Yamano, Katsuhiro; Yamamoto, Takao; Terai, Takao; Kusunoki, Takahiro; Tsubaki, Kazunori; Shiokawa, Youichi
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 6 p. 1188 - 1195
100-59-4
苯基氯化镁
→
反应条件
96306-54-6
反应条件
1: benzene / 1.) RT, 50 min, 2.) 70 deg C, 7 h 2: conc. aq. HCl / benzene; methanol; tetrahydrofuran / 7 h / Heating View Scheme
参考文献
Taniguchi, Kiyoshi; Miyao, Yasuhiro; Yamano, Katsuhiro; Yamamoto, Takao; Terai, Takao; Kusunoki, Takahiro; Tsubaki, Kazunori; Shiokawa, Youichi
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 6 p. 1188 - 1195
