4-甲基-1-硝基-2-[2-(2-硝基苯氧基)乙氧基]-苯合成路线 （共 7 条）
反应条件
potassium carbonate in DMF (N,N-dimethyl-formamide)
T=130°C; 18 h;
参考文献
MOLECULAR PROBES, INC.
Patent: WO2005/16874 A2, 2005 ;
Location in patent: Page/Page column 55-56 ;
反应条件
1: 2-hydroxy-4-methylnitrobenzene With potassium carbonate in N,N-dimethyl-formamide
T=45°C; 0.5 h;
2: 1-(2-bromoethoxy)-2-nitrobenzene in N,N-dimethyl-formamide
T=130°C; 3 h;
参考文献
Dong, Xiaohu; Yang, Yiyao; Sun, Jian; Liu, Zhihong; Liu, Bi-Feng
Chemical Communications, 2009 , # 26 p. 3883 - 3885
反应条件
potassium carbonate in N,N-dimethyl-formamide
参考文献
Molecular Probes, Inc.
Patent: US2002/164616 A1, 2002 ;
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=120°C; 1 h;
参考文献
Matsui, Akihiro; Umezawa, Keitaro; Shindo, Yutaka; Fujii, Tomohiko; Citterio, Daniel; Oka, Kotaro; Suzuki, Koji
Chemical Communications, 2011 , vol. 47, # 37 p. 10407 - 10409
反应条件
1: potassium carbonate
2: potassium carbonate
View Scheme
参考文献
Sanchez-Martin, Rosario M.; Cuttle, Matt; Mittoo, Stifun; Bradley, Mark
Angewandte Chemie - International Edition, 2006 , vol. 45, # 33 p. 5472 - 5474
反应条件
potassium carbonate
Inert atmosphere;
参考文献
Bhattacharyya, Koyel X.; Boubekeur-Lecaque, Leila; Tapsoba, Issa; Maisonhaute, Emmanuel; Schoellhorn, Bernd; Amatore, Christian
Chemical Communications, 2011 , vol. 47, # 18 p. 5199 - 5201
反应条件
hydrogen; palladium 10 on activated carbon in DMF (N,N-dimethyl-formamide)
P=2068.65 Torr; 18 h;
参考文献
MOLECULAR PROBES, INC.
Patent: WO2005/16874 A2, 2005 ;
Location in patent: Page/Page column 56 ;
