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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
96563-15-4
合成路线
（共 6 条）
96563-15-4
→
反应条件
294-92-8
4,10-二氮杂-12-冠4-醚
反应条件
lithium aluminium tetrahydride in tetrahydrofuran Reduction; 48 h; Heating;
参考文献
Quici, Silvio; Manfredi, Amedea; Maestri, Mauro; Manet, Ilse; Passaniti, Paolo; Balzani, Vincenzo
European Journal of Organic Chemistry, 2000 , # 11 p. 2041 - 2046
80639-62-9
→
反应条件
96563-15-4
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate 24 h; Ambient temperature;
参考文献
Anelli, Pier Lucio; Montanari, Fernando; Quici, Silvio; Ciani, Gianfranco; Sironi, Angelo
Journal of Organic Chemistry, 1988 , vol. 53, # 22 p. 5292 - 5298
96563-14-3
→
反应条件
96563-15-4
反应条件
sodium hydroxide in ethanol 72 h; Heating;
参考文献
Anelli, Pier Lucio; Montanari, Fernando; Quici, Silvio; Ciani, Gianfranco; Sironi, Angelo
Journal of Organic Chemistry, 1988 , vol. 53, # 22 p. 5292 - 5298
72358-83-9
→
反应条件
96563-15-4
反应条件
1: 96 percent / pyridine / 2 h / 0 °C 2: 51 percent / Na2CO3 / acetonitrile / 40 h / Heating 3: 90 percent / tetrahydrofuran / 2 h / 60 °C 4: 89 percent / aq.NaOH / ethanol / 72 h / Heating View Scheme
参考文献
Anelli, Pier Lucio; Montanari, Fernando; Quici, Silvio; Ciani, Gianfranco; Sironi, Angelo
Journal of Organic Chemistry, 1988 , vol. 53, # 22 p. 5292 - 5298
70-55-3
对甲苯磺酰胺
→
反应条件
96563-15-4
反应条件
1: 77 percent / K2CO3 / dimethylformamide / 96 h / Heating 2: 96 percent / pyridine / 2 h / 0 °C 3: 51 percent / Na2CO3 / acetonitrile / 40 h / Heating 4: 90 percent / tetrahydrofuran / 2 h / 60 °C 5: 89 percent / aq.NaOH / ethanol / 72 h / Heating View Scheme
参考文献
Anelli, Pier Lucio; Montanari, Fernando; Quici, Silvio; Ciani, Gianfranco; Sironi, Angelo
Journal of Organic Chemistry, 1988 , vol. 53, # 22 p. 5292 - 5298
80639-61-8
→
反应条件
96563-15-4
反应条件
1: 51 percent / Na2CO3 / acetonitrile / 40 h / Heating 2: 90 percent / tetrahydrofuran / 2 h / 60 °C 3: 89 percent / aq.NaOH / ethanol / 72 h / Heating View Scheme
参考文献
Anelli, Pier Lucio; Montanari, Fernando; Quici, Silvio; Ciani, Gianfranco; Sironi, Angelo
Journal of Organic Chemistry, 1988 , vol. 53, # 22 p. 5292 - 5298
