1-(2-氟-5-硝基苯基)-1H-吡咯合成路线 (共 3 条)
反应条件
in acetic acid
T=130°C; 0.5 h;
参考文献
Stefancich; Artico; Corelli; Massa; Panico; Simonetti
Farmaco, Edizione Scientifica, 1985 , vol. 40, # 4 p. 237 - 248
反应条件
1: hydrogen / 5percent rhodium on alumina / aq. ethanol / 3040 Torr
2: 80.8 percent / aq. ethanol
3: 40.4 percent / diphenyl ether / 0.5 h / Heating
4: 60.9 percent / potassium carbonate powder / dimethylformamide / 4 h / 90 °C
5: 73.3 percent / 10percent aq sodium hydroxide / ethanol; H2O / 1 h / Heating
View Scheme
参考文献
Stefancich; Artico; Corelli; Massa; Panico; Simonetti
Farmaco, Edizione Scientifica, 1985 , vol. 40, # 4 p. 237 - 248
反应条件
1: hydrogen / 5percent rhodium on alumina / aq. ethanol / 3040 Torr
2: 80.8 percent / aq. ethanol
3: 40.4 percent / diphenyl ether / 0.5 h / Heating
4: 69.9 percent / 10percent aq sodium hydroxide / ethanol / 1 h / Heating
View Scheme
参考文献
Stefancich; Artico; Corelli; Massa; Panico; Simonetti
Farmaco, Edizione Scientifica, 1985 , vol. 40, # 4 p. 237 - 248