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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
96623-78-8
合成路线
（共 5 条）
158533-30-3
→
反应条件
96623-78-8
反应条件
sodium hydroxide in ethanol 1 h; Heating;
参考文献
Stefancich; Artico; Corelli; Massa; Panico; Simonetti
Farmaco, Edizione Scientifica, 1985 , vol. 40, # 4 p. 237 - 248
369-36-8
2-氟-5-硝基苯胺
→
反应条件
96623-78-8
反应条件
1: 88.3 percent / acetic acid / 0.5 h / 130 °C 2: hydrogen / 5percent rhodium on alumina / aq. ethanol / 3040 Torr 3: 80.8 percent / aq. ethanol 4: 40.4 percent / diphenyl ether / 0.5 h / Heating 5: 69.9 percent / 10percent aq sodium hydroxide / ethanol / 1 h / Heating View Scheme
参考文献
Stefancich; Artico; Corelli; Massa; Panico; Simonetti
Farmaco, Edizione Scientifica, 1985 , vol. 40, # 4 p. 237 - 248
96623-75-5
1-(2-氟-5-硝基苯基)-1H-吡咯
→
反应条件
96623-78-8
反应条件
1: hydrogen / 5percent rhodium on alumina / aq. ethanol / 3040 Torr 2: 80.8 percent / aq. ethanol 3: 40.4 percent / diphenyl ether / 0.5 h / Heating 4: 69.9 percent / 10percent aq sodium hydroxide / ethanol / 1 h / Heating View Scheme
参考文献
Stefancich; Artico; Corelli; Massa; Panico; Simonetti
Farmaco, Edizione Scientifica, 1985 , vol. 40, # 4 p. 237 - 248
96623-76-6
→
反应条件
96623-78-8
反应条件
1: 40.4 percent / diphenyl ether / 0.5 h / Heating 2: 69.9 percent / 10percent aq sodium hydroxide / ethanol / 1 h / Heating View Scheme
参考文献
Stefancich; Artico; Corelli; Massa; Panico; Simonetti
Farmaco, Edizione Scientifica, 1985 , vol. 40, # 4 p. 237 - 248
96623-78-8
→
反应条件
91524-15-1
伊洛沙星
反应条件
1: 70 percent / potassium carbonate powder / dimethylformamide / 5 h / 80 - 90 °C 2: 73.3 percent / 10percent aq sodium hydroxide / ethanol; H2O / 1 h / Heating View Scheme
参考文献
Stefancich; Artico; Corelli; Massa; Panico; Simonetti
Farmaco, Edizione Scientifica, 1985 , vol. 40, # 4 p. 237 - 248
