1-溴-4-(正辛氧基)苯合成路线 (共 15 条)
反应条件
potassium carbonate Williamson's etherification;
参考文献
Nassif, Larissa; Jakli, Antal; Seed, Alexander J.
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 2001 , vol. 365, p. 171 - 179
反应条件
sodium chlorite; silica gel; Mn(III) acetylacetonate; sodium bromide in dichloromethane T=25°C; 2 h;
参考文献
Hirano, Masao; Monobe, Hiroyuki; Yakabe, Shigetaka; Morimoto, Takashi
Synthetic Communications, 1998 , vol. 28, # 8 p. 1463 - 1470
反应条件
18-crown-6 ether; potassium carbonate in tetrahydrofuran 48 h; Heating;
参考文献
Bronk, Krys; Thayumanavan
Journal of Organic Chemistry, 2003 , vol. 68, # 14 p. 5559 - 5567
参考文献
Kanto Kagaku Kabushiki Kaisha
Patent: US5382380 A1, 1995 ;
反应条件
di-isopropyl azodicarboxylate; triphenylphosphine in tetrahydrofuran
参考文献
Chemical Communications, , vol. 49, # 74 p. 8202 - 8204
反应条件
Yield givenMultistep reaction;
参考文献
Furuta, Satoru; Kuroboshi, Manabu; Hiyama, Tamejiro
Bulletin of the Chemical Society of Japan, 1999 , vol. 72, # 4 p. 805 - 819
反应条件
magnesium 1.) Et2O, r.t., 3 h; reflux, 2 h, 2.) ether, r.t., 2 h; Multistep reaction;
参考文献
Kaspar; Sverenyak; Hamplova; Pakhomov; Glogarova
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 1995 , vol. 260, # pt 1 p. 241 - 246
反应条件
1: With n-butyllithium; boric acid trimethyl ester 2: With hydrogenchloride
参考文献
Nassif, Larissa; Jakli, Antal; Seed, Alexander J.
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 2001 , vol. 365, p. 171 - 179
反应条件
magnesium in tetrahydrofuran
参考文献
Hoechst Aktiengesellschaft
Patent: US5629428 A1, 1997 ;
反应条件
hydrogenchloride in tetrahydrofuran; hexane
参考文献
Secretary of State for Defence in Her Britannic Majesty's Government of the United Kingdom of Great Britain and Northern Ireland
Patent: US5853613 A1, 1998 ;