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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
96898-10-1
合成路线
（共 16 条）
77902-90-0
L-2-((三氟甲基磺酰基)氧基)丙酸乙酯
+
96898-10-1
→
反应条件
1006904-68-2
+
349-43-9
2-氟丙酸乙酯
反应条件
in acetonitrile T=20°C; 12 h;
参考文献
Tetrahedron Letters, , vol. 49, # 3 p. 449 - 454
17151-49-4
+
96898-10-1
→
反应条件
407-14-7
1-溴-4-三氟甲氧基苯
反应条件
1: With trifluoromethanesulfonic acid trifluoromethyl ester; sodium hydrogencarbonate in tetrahydrofuran T=-30°C; Inert atmosphere; 2: With AgPF6; F-TEDA-PF6 in tetrahydrofuran; acetone T=-30 - 23°C; Inert atmosphereDarkness;
参考文献
Huang, Chenghong; Liang, Theresa; Harada, Shinji; Lee, Eunsung; Ritter, Tobias
Journal of the American Chemical Society, 2011 , vol. 133, # 34 p. 13308 - 13310
1765-93-1
4-氟苯硼酸
+
96898-10-1
→
反应条件
352-67-0
4-三氟甲氧基氟苯
反应条件
1: 4-fluorophenyl boronic acid With sodium hydroxide in methanol T=23°C; 0.25 h; Inert atmosphere; 2: With AgPF6 in methanol T=0°C; 0.5 h; Inert atmosphere; 3: tris(dimethylamino)sulfonium trifluoromethoxide Further stages;
参考文献
Huang, Chenghong; Liang, Theresa; Harada, Shinji; Lee, Eunsung; Ritter, Tobias
Journal of the American Chemical Society, 2011 , vol. 133, # 34 p. 13308 - 13310
17151-47-2
4-氟三丁基甲锡烷基苯
+
96898-10-1
→
反应条件
352-67-0
4-三氟甲氧基氟苯
反应条件
1: With trifluoromethanesulfonic acid trifluoromethyl ester; tris(dimethylamino)-sulphonium difluorotrimethylsilicate; sodium hydrogencarbonate in tetrahydrofuran T=-50°C; Inert atmosphere; 2: With AgPF6; F-TEDA-PF6 in tetrahydrofuran; acetone T=-50 - 23°C; Inert atmosphereDarkness;
参考文献
Huang, Chenghong; Liang, Theresa; Harada, Shinji; Lee, Eunsung; Ritter, Tobias
Journal of the American Chemical Society, 2011 , vol. 133, # 34 p. 13308 - 13310
17151-47-2
4-氟三丁基甲锡烷基苯
+
96898-10-1
→
反应条件
462-06-6
氟苯
+
371-41-5
4-氟苯酚
+
352-67-0
4-三氟甲氧基氟苯
反应条件
1: With trifluoromethanesulfonic acid trifluoromethyl ester; sodium hydrogencarbonate in tetrahydrofuran T=-30°C; Inert atmosphere; 2: With silver nitrate; F-TEDA-PF6 in tetrahydrofuran; acetone T=-30 - 23°C; Inert atmosphereDarkness;
参考文献
Journal of the American Chemical Society, , vol. 133, # 34 p. 13308 - 13310
→
反应条件
212695-45-9
6-(三氟甲氧基)喹啉
反应条件
1: tris(dimethylamino)sulfonium trifluoromethoxide With trifluoromethanesulfonic acid trifluoromethyl ester; sodium hydrogencarbonate in tetrahydrofuran T=-50°C; Inert atmosphere; 2: 6-(tributylstannyl)quinoline With AgPF6; F-TEDA-PF6 in tetrahydrofuran; acetone T=-30 - 23°C; Inert atmosphereDarkness;
参考文献
Huang, Chenghong; Liang, Theresa; Harada, Shinji; Lee, Eunsung; Ritter, Tobias
Journal of the American Chemical Society, 2011 , vol. 133, # 34 p. 13308 - 13310
17151-47-2
4-氟三丁基甲锡烷基苯
+
96898-10-1
→
反应条件
462-06-6
氟苯
+
371-41-5
4-氟苯酚
+
352-67-0
4-三氟甲氧基氟苯
反应条件
1: With trifluoromethanesulfonic acid trifluoromethyl ester; sodium hydrogencarbonate in tetrahydrofuran T=-30°C; Inert atmosphere; 2: With silver nitrate; F-TEDA-PF6 in tetrahydrofuran; acetone T=-30 - 23°C; Inert atmosphereDarkness;
参考文献
Huang, Chenghong; Liang, Theresa; Harada, Shinji; Lee, Eunsung; Ritter, Tobias
Journal of the American Chemical Society, 2011 , vol. 133, # 34 p. 13308 - 13310
17151-47-2
4-氟三丁基甲锡烷基苯
+
96898-10-1
→
反应条件
462-06-6
氟苯
+
371-41-5
4-氟苯酚
+
352-67-0
4-三氟甲氧基氟苯
反应条件
1: With trifluoromethanesulfonic acid trifluoromethyl ester; sodium hydrogencarbonate in tetrahydrofuran T=-30°C; Inert atmosphere; 2: With silver nitrate; F-TEDA-PF6 in tetrahydrofuran; acetone T=-30 - 23°C; Inert atmosphereDarkness;
参考文献
Huang, Chenghong; Liang, Theresa; Harada, Shinji; Lee, Eunsung; Ritter, Tobias
Journal of the American Chemical Society, 2011 , vol. 133, # 34 p. 13308 - 13310
70744-47-7
三丁基(4-甲氧基苯基)锡
+
96898-10-1
→
反应条件
710-18-9
4-(三氟甲氧基)苯甲醚
反应条件
1: With trifluoromethanesulfonic acid trifluoromethyl ester; sodium hydrogencarbonate in tetrahydrofuran T=-30°C; Inert atmosphere; 2: With AgPF6; F-TEDA-PF6 in tetrahydrofuran; acetone T=-30 - 23°C; Inert atmosphereDarkness;
参考文献
Huang, Chenghong; Liang, Theresa; Harada, Shinji; Lee, Eunsung; Ritter, Tobias
Journal of the American Chemical Society, 2011 , vol. 133, # 34 p. 13308 - 13310
5720-07-0
4-甲氧基苯硼酸
+
96898-10-1
→
反应条件
710-18-9
4-(三氟甲氧基)苯甲醚
反应条件
1: (4-methoxyphenyl)-boronic acid With sodium hydroxide in methanol T=23°C; 0.25 h; Inert atmosphere; 2: With AgPF6 in methanol T=0°C; 0.5 h; Inert atmosphere; 3: tris(dimethylamino)sulfonium trifluoromethoxide Further stages;
参考文献
Huang, Chenghong; Liang, Theresa; Harada, Shinji; Lee, Eunsung; Ritter, Tobias
Journal of the American Chemical Society, 2011 , vol. 133, # 34 p. 13308 - 13310
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