3-(2-甲氧基苯基)苯胺合成路线 (共 9 条)
反应条件
potassium carbonate; Pd0(tris(tert-butyl)phosphine)2 in methanol; water; toluene T=135°C; 0.583333 h; Irradiation;
参考文献
ASTEX THERAPEUTICS LIMITED
Patent: WO2007/72041 A1, 2007 ;
Location in patent: Page/Page column 68 ;
WO 2007/072041 A1
反应条件
potassium phosphate; bis(dicyclohexylamine)-palladium(II) acetate in ethanol T=20°C; Suzuki reaction; 4 h;
参考文献
Tao, Bin; Boykin, David W.
Journal of Organic Chemistry, 2004 , vol. 69, # 13 p. 4330 - 4335
反应条件
hydrogen; palladium on activated charcoal P=2585.7 Torr; 3 h;
参考文献
Beadle, James R.; Dishong, Dennis M.; Khanna, Raj K.; Gokel, George W.
Tetrahedron, 1984 , vol. 40, # 20 p. 3935 - 3944
反应条件
1: 35 percent / potassium acetate / 12 h 2: 88 percent / H2 / 10percent Pd/C / 3 h / 2585.7 Torr View Scheme
参考文献
Tetrahedron, , vol. 40, # 20 p. 3935 - 3944
反应条件
1: 35 percent / potassium acetate / 12 h 2: 88 percent / H2 / 10percent Pd/C / 3 h / 2585.7 Torr View Scheme
参考文献
Tetrahedron, , vol. 40, # 20 p. 3935 - 3944
反应条件
1: sodium acetate / <10 2: Raney nickel; ethanol / Hydrogenation View Scheme
参考文献
Journal and Proceedings of the Royal Society of New South Wales, , vol. 80, p. 77,79
反应条件
1: Na2SO4 2: Raney nickel; ethanol / Hydrogenation View Scheme
参考文献
Journal and Proceedings of the Royal Society of New South Wales, , vol. 80, p. 77,79
反应条件
1: sodium acetate; acetic acid anhydride / 20 °C / anschliessendes Erwaermen auf 80grad 2: Raney nickel; ethanol / Hydrogenation View Scheme
参考文献
Journal and Proceedings of the Royal Society of New South Wales, , vol. 80, p. 77,79
反应条件
hydrogenchloride; potassium hypophosphite T=0°C; Diazotization;
参考文献
Dunstan; Hughes
Journal and Proceedings of the Royal Society of New South Wales, 1946 , vol. 80, p. 77,79