2,3-二氯-4-氟代-N-乙酰苯胺合成路线 （共 9 条）
反应条件
triethylamine in dichloromethane T=0 - 25°C;
参考文献
Ma, Liang; Li, Shilin; Zheng, Hao; Chen, Jinying; Lin, Lin; Ye, Xia; Chen, Zhizhi; Xu, Qinyuan; Chen, Tao; Yang, Jincheng; Qiu, Neng; Wang, Guangcheng; Peng, Aihua; Ding, Yi; Wei, Yuquan; Chen, Lijuan
European Journal of Medicinal Chemistry, 2011 , vol. 46, # 6 p. 2003 - 2010
反应条件
1: 80 percent / K2CO3 / acetone / 4 h / Heating 2: 60 percent / Lawesson's reagent / toluene / 2 h / Heating 3: K2CO3 / acetone / 4 h / Heating 4: dimethylformamide / 6 h / Heating View Scheme
参考文献
Bansal, O P; Srinivas, J S; Sastry, C V Reddy
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 4 p. 289 - 292
反应条件
1: 75 percent / K2CO3 / acetone / 4 h / Heating 2: 90 percent / Lawesson's reagent / toluene / 2 h / Heating 3: K2CO3 / acetone / 4 h / Heating 4: dimethylformamide / 6 h / Heating View Scheme
参考文献
Bansal, O P; Srinivas, J S; Sastry, C V Reddy
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 4 p. 289 - 292
反应条件
1: 75 percent / K2CO3 / acetone / 4 h / Heating 2: 90 percent / Lawesson's reagent / toluene / 2 h / Heating 3: K2CO3 / acetone / 4 h / Heating 4: dimethylformamide / 6 h / Heating View Scheme
参考文献
Bansal, O P; Srinivas, J S; Sastry, C V Reddy
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 4 p. 289 - 292
反应条件
1: 80 percent / K2CO3 / acetone / 4 h / Heating 2: 60 percent / Lawesson's reagent / toluene / 2 h / Heating 3: K2CO3 / acetone / 4 h / Heating 4: dimethylformamide / 6 h / Heating View Scheme
参考文献
Bansal, O P; Srinivas, J S; Sastry, C V Reddy
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 4 p. 289 - 292
反应条件
1: 75 percent / K2CO3 / acetone / 4 h / Heating 2: 90 percent / Lawesson's reagent / toluene / 2 h / Heating 3: K2CO3 / acetone / 4 h / Heating 4: dimethylformamide / 6 h / Heating View Scheme
参考文献
Bansal, O P; Srinivas, J S; Sastry, C V Reddy
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 4 p. 289 - 292
反应条件
1: 75 percent / K2CO3 / acetone / 4 h / Heating 2: 90 percent / Lawesson's reagent / toluene / 2 h / Heating 3: K2CO3 / acetone / 4 h / Heating 4: dimethylformamide / 6 h / Heating View Scheme
参考文献
Bansal, O P; Srinivas, J S; Sastry, C V Reddy
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 4 p. 289 - 292
反应条件
pyridine; hydrogenchloride; magnesium sulfate; aluminium trichloride in toluene
参考文献
Pfizer Inc.
Patent: US4725616 A1, 1988 ;
反应条件
1: 80 percent / K2CO3 / acetone / 4 h / Heating 2: 60 percent / Lawesson's reagent / toluene / 2 h / Heating 3: K2CO3 / acetone / 4 h / Heating 4: dimethylformamide / 6 h / Heating View Scheme
参考文献
Bansal, O P; Srinivas, J S; Sastry, C V Reddy
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 4 p. 289 - 292
