1-氯-2,4-二硝基苯合成路线 （共 755 条）
反应条件
1: propanol-(1) 2: sodium disulfide; water 3: diluted aqueous HCl / Diazotization.Behandlung mit CuCl in wss. HCl, zuletzt bei 60grad, und Kochen des Reaktionsprodukts mit AlCl3 in Benzol View Scheme
参考文献
Verkade; van Dijk; Meerburg
Recueil des Travaux Chimiques des Pays-Bas, 1946 , vol. 65, p. 346,350, 357
反应条件
sulfuric acid; nitric acid
参考文献
Chem. Fabr. Griesheim
Patent: DE78309 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 4, p. 35
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Giua; de Franciscis
Ann. Chim. applic., vol. 15, p. 141
Chem. Zentralbl., 1926 , vol. 97, # I p. 225
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Frankland; Garner
Journal of the Society of Chemical Industry, London, 1920 , vol. 39, p. 257 T
Chem. Zentralbl., 1920 , vol. 91, # III p. 792
反应条件
sulfur trioxide; nitric acid in sulfuric acid T=130°C; 0.5 h; isotope labelled experiments; Product distributionRate constantMechanism;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1637 - 1642
反应条件
hydrogenchloride; sulfuric acid; nitric acid T=130°C; Cl2 in place of HCl; Rate constantProduct distribution;
参考文献
Melhuish, Martin W.; Moodie, Roy B.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 667 - 674
反应条件
hydrogen; potassium acetate; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=100°C; 2 h;
参考文献
Akitta, Yasuo; Inoue, Akira; Ishida, Keiko; Terui, Kiyoko; Ohta, Akihiro
Synthetic Communications, 1986 , vol. 16, # 9 p. 1067 - 1072
反应条件
isobutyramide; copper T=100°C; 4 h;
参考文献
Clark, James H.; Denness, James E.; McClinton, Martin A.; Wynd, Andrew J.
Journal of Fluorine Chemistry, 1990 , vol. 50, # 3 p. 411 - 426
参考文献
Smith
Journal of the American Chemical Society, 1949 , vol. 71, p. 2855
反应条件
in methanol T=65°C; 10 h; other solvent, temperature,time. Dependence of the degree of conversion on the reaction time in methanol at 130 deg C.; Product distribution;
参考文献
Plakidin, Val. L.; Vostrova, V. N.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 295 - 303
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 2 p. 342 - 352
反应条件
in methanol T=65°C; 10 h; Product distribution;
参考文献
Plakidin, Val. L.; Vostrova, V. N.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 295 - 303
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 2 p. 342 - 352
反应条件
in 1,4-dioxane; water T=45°C; 0.5 h; other temperatures; KineticsThermodynamic dataProduct distribution;
参考文献
Ikramuddeen; Chandrasekara; Ramarajan; Subramania n
Journal of the Indian Chemical Society, 1989 , vol. 66, # 5 p. 342 - 344
