1-氯-2,4-二硝基苯合成路线 (共 755 条)
反应条件
1.1: acetone / |Reflux 2.1: aniline / ethanol / 0.08 h / 20 °C 2.2: 20 °C View Scheme
参考文献
Okoh, Okoh Adeyi; Bisby, Roger H.; Lawrence, Clare L.; Rolph, Carole E.; Smith, Robert B.
Journal of Sulfur Chemistry, 2014 , vol. 35, # 1 p. 42 - 56
反应条件
in dichloromethane T=20°C; 12 h; other sodium alkyl peroxide, other halonitroaromatic compounds, also in presence of crown ethers and NaOH, var. time; Mechanism;
参考文献
Polish Journal of Chemistry, , vol. 67, # 11 p. 1967 - 1972
参考文献
Ostromysslenski
Journal fuer Praktische Chemie (Leipzig), 1908 , vol. <2> 78, p. 261
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Jungfleisch
Annales de Chimie (Cachan, France), 1868 , vol. <4> 15, p. 234,238
Jahresbericht ueber die Fortschritte der Chemie und Verwandter Theile Anderer Wissenschaften, 1868 , p. 346
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Claus; Stiebel
Chemische Berichte, 1887 , vol. 20, p. 1379
反应条件
thiourea in sulpholane (tetrahydrothiophene 1,1-dioxide); water
参考文献
Bayer Aktiengesellschaft
Patent: US4808723 A1, 1989 ;
反应条件
in tetramethylene sulfide; water
参考文献
Bayer Aktiengesellschaft
Patent: US4808723 A1, 1989 ;
反应条件
pyridine 3 h; Reflux;
参考文献
Palkar, Mahesh; Noolvi, Malleshappa; Sankangoud, Ramappa; Maddi, Veeresh; Gadad, Andanappa; Nargund, Laxmi Venkat G.
Archiv der Pharmazie, 2010 , vol. 343, # 6 p. 353 - 359
反应条件
1: 68 percent / pyridine / methanol / 3 h / Heating 2: 75 percent / ammonium chloride, ammonium carbonate, ammonia soln., sodium sulphide / H2O / 1 h / 60 °C View Scheme
参考文献
Devi; Achaiah; Malla Reddy
Journal of the Indian Chemical Society, 1988 , vol. 65, # 8 p. 567 - 570
反应条件
isopropyl alcohol; potassium hydroxide 0.166667 h; Microwave irradiation; regioselective reaction;
参考文献
Farhadi, Saeid; Siadatnasab, Firouzeh
Journal of Molecular Catalysis A: Chemical, 2011 , vol. 339, # 1-2 p. 108 - 116
反应条件
hydrogen; iron; acetic acid; palladium dichloride in ethanol T=20 - 25°C; P=258.6 - 2327.2 Torr;
参考文献
Theodoridis; Manfredi; Krebs
Tetrahedron Letters, 1990 , vol. 31, # 43 p. 6141 - 6144
反应条件
hydrogen; Pt/γ-Fe2O3 nanocomposite in methanol T=29.84°C; P=75.0075 Torr; Product distribution;
参考文献
Liang, Minghui; Wang, Xiaodong; Liu, Hongquan; Liu, Haichao; Wang, Yuan
Journal of Catalysis, 2008 , vol. 255, # 2 p. 335 - 342