1-氯-2,4-二硝基苯合成路线 (共 755 条)
反应条件
sodium hydroxide in water variation of surfactants and hydroxide ion concentration; Rate constant;
参考文献
Crampton, Michael R.; Davis, Antony B.; Greenhalgh, Colin; Stevens, J. Andrew
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 675 - 682
反应条件
N-hexadecyl-N,N,N-trimethylammonium bromide in octane; water T=25°C; KineticsProduct distribution;
参考文献
Athanassakis, Vassilios; Bunton, Clifford A.; Buzzaccarini, Francesco de
Journal of Physical Chemistry, 1982 , vol. 86, # 25 p. 5002 - 5009
反应条件
sodium hydride; 3-methylthio-5-amino-1H-1,2,4-triazole 1.) DMF, 0 deg C, 1 h, 2.) DMF, 60 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Trinka, Peter; Reiter, Jozsef
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 4 p. 1359 - 1372
反应条件
sodium hydride; 3-methylthio-5-amino-1H-1,2,4-triazole 1.) 0 deg C, 1 h, 2.) 60 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Trinka, Peter; Reiter, Jozsef
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 4 p. 1359 - 1372
反应条件
sodium hydride 1.) DMF, 0 deg C, 1 h, 2.) DMF, 60 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Trinka, Peter; Reiter, Jozsef
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 4 p. 1359 - 1372
反应条件
sodium hydride 1.) DMF, 0 deg C, 1 h, 2.) DMF, 60 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Trinka, Peter; Reiter, Jozsef
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 4 p. 1359 - 1372
反应条件
sodium carbonate in ethanol 12 h; Heating;
参考文献
Henichart, J. P.; Bernier J. L.; Vaccher, C.; Houssin, R.; Warin, V.; Baert, F.
Tetrahedron, 1980 , vol. 36, p. 3535 - 3542
反应条件
pyridine 12 h; Heating;
参考文献
Tetrahedron, , vol. 36, p. 3535 - 3542
反应条件
1: aqueous NaHS / anschliessend mit CS2 2: KMnO4; aqueous H2SO4 3: SnCl2; tin; aqueous HCl View Scheme
参考文献
Helvetica Chimica Acta, , vol. 33, p. 1429,1431
反应条件
sodium ethanolate in ethanol; acetonitrile
参考文献
Ciba-Geigy
Patent: US3941832 , 1976 ;
Chem.Abstr., 1977 , vol. 86, # 5159
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Ciba-Geigy
Patent: US3941839 , 1976 ;
Chem.Abstr., 1977 , vol. 86, # 5160