1-氯-2,4-二硝基苯合成路线 （共 755 条）
反应条件
1: aq.-ethanolic ammonia; hydrazine hydrate View Scheme
参考文献
Brady
Journal of the Chemical Society, 1931 , p. 756,758
反应条件
in benzene T=22°C; Rate constant;
参考文献
Um, Ik-Hwan; Im, Li-Ra; Kang, Ji-Sun; Bursey, Samantha S.; Dust, Julian M.
Journal of Organic Chemistry, 2012 , vol. 77, # 21 p. 9738 - 9746
反应条件
1: diluted alcohol View Scheme
参考文献
Allen
Journal of the American Chemical Society, 1930 , vol. 52, p. 2956
Organic Syntheses, 1943 , vol. Coll. Vol. II, p. 228
参考文献
Ciusa
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1909 , vol. <5> 18 II, p. 66
反应条件
hydrazine hydrate in ethanol 3.5 h; Reflux;
参考文献
Furmansky, Yulia; Sasson, Hela; Liddell, Paul; Gust, Devens; Ashkenasy, Nurit; Visoly-Fisher, Iris
Journal of Materials Chemistry, 2012 , vol. 22, # 38 p. 20334 - 20341
参考文献
Allen
Journal of the American Chemical Society, 1930 , vol. 52, p. 2956
Organic Syntheses, 1943 , vol. Coll. Vol. II, p. 228
反应条件
1: tin dichloride; hydrochloric acid 2: durch Austausch der NH2-Gruppen gegen Chlor nach dem Sandmeyerschen Verfahren View Scheme
参考文献
Cohn; Fischer
Monatshefte fuer Chemie, 1900 , vol. 21, p. 268
反应条件
1: 1.) cumene hydroperoxide, NaOH, 2.) sodium hypophosphite / 1.) CH2Cl2, liquid NH3, -33 deg C, 1 h, 2.) -10 deg C; room temperature, 4 h 2: 1.) H2, conc. HCl, 2.) stannous chloride dihydrate, conc. HCl / 1.) 10percent Pd/C / 1.) H2O, 55 deg C, 4 h, 2.) 25 deg C 3: 94 percent / conc. HCl / 18 h / 150 °C View Scheme
参考文献
Pews, R. Garth; Lysrnko, Zenon; Vosejpka, Paul C.
Journal of Organic Chemistry, 1997 , vol. 62, # 23 p. 8255 - 8256
参考文献
Clariant Finance (BVI) Limited
Patent: EP731146 A2, 1996 ;
反应条件
sodium hydrogencarbonate in ethanol 4 h; Heating;
参考文献
Adegoke, E. A.; Alo, Babajide I.; Ogunsulire, F. O.
Journal of Heterocyclic Chemistry, 1982 , vol. 19, p. 1169 - 1172
