1-氯-2,4-二硝基苯合成路线 (共 755 条)
反应条件
1: diluted alcohol View Scheme
参考文献
Allen
Journal of the American Chemical Society, 1930 , vol. 52, p. 2956
Organic Syntheses, 1943 , vol. Coll. Vol. II, p. 228
反应条件
1: aq.-ethanolic ammonia; hydrazine hydrate View Scheme
参考文献
Brady
Journal of the Chemical Society, 1931 , p. 756,758
反应条件
triphenylphosphine; [(CO)4Fe(μ-PPh2)Pd(μ-Cl)]2 in benzene T=78°C; 16 h;
参考文献
Shenglof, Margarita; Gelman, Dmitri; Heymer, Bernd; Schumann, Herbert; Molander, Gary A.; Blum, Jochanan
Synthesis, 2003 , # 2 p. 302 - 306
反应条件
2: 70 percent / HCl gas / POCl3 / 1.5 h / Heating 3: 68 percent / NH2NH2*H2O / glycerol / 6 h / Heating 4: 60 percent / dioxane / 4 h / Heating 6: 67 percent / C2H5OCSS(-)K(+) / H2O / 0 °C View Scheme
参考文献
Joshi; Barar
Pharmazie, 1989 , vol. 44, # 4 p. 265 - 267
反应条件
1: alcohol; hydrazine hydrate 2: acetic acid View Scheme
参考文献
Purgotti
Gazzetta Chimica Italiana, 1894 , vol. 24 I, p. 568
反应条件
ethanol; sodium hydrogencarbonate
参考文献
Abderhalden; Stix
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1923 , vol. 129, p. 145,150
参考文献
Abderhalden; Stix
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1923 , vol. 129, p. 145,150
反应条件
1: 78 percent / sodium hydrogen carbonate / ethanol / 2 h / Heating 2: 56 percent / piperidine / ethanol / 2 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 681 - 690
反应条件
in benzene T=40°C; other solvent; Rate constantMechanism;
参考文献
Forlani, Luciano
Gazzetta Chimica Italiana, 1982 , vol. 112, # 5/6 p. 205 - 212
反应条件
in 1,4-dioxane; water T=45°C; 0.5 h; other temperatures; KineticsThermodynamic dataProduct distribution;
参考文献
Ikramuddeen; Chandrasekara; Ramarajan; Subramania n
Journal of the Indian Chemical Society, 1989 , vol. 66, # 5 p. 342 - 344