1-氯-2,4-二硝基苯合成路线 （共 755 条）
反应条件
sodium azide; sodium L-ascorbate; phenylacetylene in water; tert-butyl alcohol
2.5 h; Heating;
参考文献
Jain, Manvi; Sharma, Maneesh; Gaur, Manoj; Ashok, Tara Devi S.; Dureja; Eswaran
Journal of the Indian Chemical Society, 2011 , vol. 88, # 4 p. 543 - 546
反应条件
in benzene
T=60°C; Title compound not separated from byproducts;
参考文献
Nudelman, N. Sbarbati; Socolovsky, S. E.
Tetrahedron Letters, 1980 , vol. 21, p. 3331 - 3334
反应条件
in benzene
T=60°C; Mechanism;
参考文献
Nudelman, N. Sbarbati; Socolovsky, S. E.
Tetrahedron Letters, 1980 , vol. 21, p. 3331 - 3334
参考文献
Crampton, Michael R.; Wilson, Penelope M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 1854 - 1858
反应条件
1: alcohol; hydrazine hydrate
View Scheme
参考文献
Purgotti
Gazzetta Chimica Italiana, 1894 , vol. 24 I, p. 568
反应条件
1: alcohol; ammonia / beim Stehen
2: beim Bromieren
3: aqueous KOH-solution
View Scheme
参考文献
Koerner
Gazzetta Chimica Italiana, 1874 , vol. 4, p. 341
Jahresbericht ueber die Fortschritte der Chemie und Verwandter Theile Anderer Wissenschaften, 1875 , p. 317
反应条件
air; tetrabutylammomium bromide; potassium carbonate; [Pd(Cl)κ2N,C,-CH2C6H2(4,6-Me)2CH=NC6H3(2,6-iPr)2]2 in water
Suzuki-Miyaura coupling reaction; 3 h; Heating;
参考文献
Chen, Chuan-Lin; Liu, Yi-Hung; Peng, Shie-Ming; Liu, Shiuh-Tzung
Tetrahedron Letters, 2005 , vol. 46, # 3 p. 521 - 523
反应条件
palladium 10 on activated carbon; lithium chloride in 1-methyl-pyrrolidin-2-one
T=120°C; Stille coupling; 24 h;
参考文献
Yabe, Yuki; Maegawa, Tomohiro; Monguchi, Yasunari; Sajiki, Hironao
Tetrahedron, 2010 , vol. 66, # 45 p. 8654 - 8660
反应条件
copper
T=210 - 230°C;
参考文献
Forrest,J.
Journal of the Chemical Society, 1960 , p. 566 - 573
反应条件
sodium hydroxide in ethanol
0.166667 h; Heating;
参考文献
Messinger, Paul; Kunick, Conrad
Synthesis, 1986 , # 3 p. 213 - 214
