1-氯-2,4-二硝基苯合成路线 （共 755 条）
反应条件
copper(l) iodide in N,N-dimethyl-formamide
T=45°C; 8 h;
参考文献
Long, Zheng-Yu; Duan, Jian-Xin; Lin, Yuan-Bin; Guo, Cai-Yun; Chen, Qing-Yun
Journal of Fluorine Chemistry, 1996 , vol. 78, # 2 p. 177 - 181
反应条件
isobutyramide; copper
T=100°C; 4 h;
参考文献
Clark, James H.; Denness, James E.; McClinton, Martin A.; Wynd, Andrew J.
Journal of Fluorine Chemistry, 1990 , vol. 50, # 3 p. 411 - 426
反应条件
1: Zn(CF3)Br*2DMF With copper(I) bromide in N,N-dimethyl-formamide
T=20°C; 3 h;
2: 1-chloro-2,4-dinitro-benzene in N,N-dimethyl-formamide
T=85 - 90°C; 8 h;
参考文献
Kremlev, Mikhail M.; Tyrra, Wieland; Mushta, Aleksej I.; Naumann, Dieter; Yagupolskii, Yurii L.
Journal of Fluorine Chemistry, 2010 , vol. 131, # 2 p. 212 - 216
反应条件
copper; carbon in N,N-dimethyl acetamide
T=100°C; 2 h;
参考文献
Clark, James H.; McClinton, Martin A.; Jones, Craig W.; Landon, Philip; Bishop, D.; Blade, R. J.
Tetrahedron Letters, 1989 , vol. 30, # 16 p. 2133 - 2136
反应条件
potassium fluoride; copper(l) iodide in N,N-dimethyl-formamide
T=100°C; 8 h; Yield given;
参考文献
Duan, Jian-Xing; Su, De-Bao; Wu, Jian-Ping; Chen, Qing-Yun
Journal of Fluorine Chemistry, 1994 , vol. 66, # 2 p. 167 - 170
反应条件
potassium fluoride; copper(l) iodide in N,N-dimethyl-formamide
T=90°C; 9 h; Yield given;
参考文献
Duan, Jian-Xing; Su, De-Bao; Wu, Jian-Ping; Chen, Qing-Yun
Journal of Fluorine Chemistry, 1994 , vol. 66, # 2 p. 167 - 170
反应条件
copper(l) iodide in N,N-dimethyl-formamide
T=70 - 80°C; 8 h; Yield given;
参考文献
Duan, Jian-Xing; Su, De-Bao; Wu, Jian-Ping; Chen, Qing-Yun
Journal of Fluorine Chemistry, 1994 , vol. 66, # 2 p. 167 - 170
反应条件
sodium hydride in N,N-dimethyl-formamide
0.5 h;
参考文献
Hagishino, Takeo; Sato, Susumu; Miyashita, Akira; Katori, Tatsuhiko
Chemical & Pharmaceutical Bulletin, 1987 , vol. 35, # 10 p. 4078 - 4086
反应条件
1: diluted alcohol
2: alcoholic hydrochloric acid
View Scheme
参考文献
Giua; Petronio
Journal fuer Praktische Chemie (Leipzig), 1925 , vol. <2> 110, p. 304
反应条件
sodium ethanolate in ethanol
T=110°C; other temperatures; ΔE(excit.), ΔG(excit.), ΔS(excit.); KineticsThermodynamic data;
参考文献
Miller, Joseph; Miyata, Yukino; Sakazaki, Emika; Witkowski De Santos, Terezinha
Journal of Chemical Research, Miniprint, 1986 , # 11 p. 3301 - 3310
