1-氯-2,4-二硝基苯合成路线 (共 755 条)
参考文献
Miller, Joseph; Miyata, Yukino; Sakazaki, Emika; Witkowski De Santos, Terezinha
Journal of Chemical Research, Miniprint, 1986 , # 11 p. 3301 - 3310
反应条件
2: aq. H2O2, AcOH
View Scheme
参考文献
Cogolli,P. et al.
Journal of Organic Chemistry, 1979 , vol. 44, # 15 p. 2636 - 2642
反应条件
2: aq. H2O2, AcOH
View Scheme
参考文献
Cogolli,P. et al.
Journal of Organic Chemistry, 1979 , vol. 44, # 15 p. 2636 - 2642
参考文献
Le Fevre; Turner
Journal of the Chemical Society, 1927 , p. 1117
反应条件
copper; nitrobenzene
T=160 - 165°C;
参考文献
Stearns; Adams
Journal of the American Chemical Society, 1930 , vol. 52, p. 2070,2073, 2074
反应条件
1: 2,4-diamino-toluene; potassium carbonate; copper(I) bromide / 1-methyl-pyrrolidin-2-one / 1 h / 110 °C / Inert atmosphere
2: boron tribromide / dichloromethane / 3 h / 0 - 20 °C
View Scheme
参考文献
Chen, Zheng; Wu, Yiran; Liu, Ying; Yang, Suijia; Chen, Yunjie; Lai, Luhua
Journal of Medicinal Chemistry, 2011 , vol. 54, # 10 p. 3650 - 3660
反应条件
potassium carbonate; butanone
参考文献
Walter
Barell-Festschr. <Basel 1936> S. 266, 271, 273
反应条件
1: alcohol; hydrazine hydrate
2: alcohol; concentrated hydrochloric acid
View Scheme
参考文献
Buelow; Seidel
Justus Liebigs Annalen der Chemie, 1924 , vol. 439, p. 53
反应条件
in acetone
Condensation; 15 h; Heating;
参考文献
Nimkar, Sandeep K.; Anderson, Andrea H.; Rimoldi, John M.; Stanton, Matthew; Castagnoli, Kay P.; Mabic, Stephane; Wang; Castagnoli Jr., Neal
Chemical Research in Toxicology, 1996 , vol. 9, # 6 p. 1013 - 1022
反应条件
in ethylene glycol
T=120°C; 6 h; Product distribution / selectivity;
参考文献
FUJI PHOTO FILM CO., LTD.
Patent: WO2005/95342 A1, 2005 ;
Location in patent: Page/Page column 27-28 ;