1-氯-2,4-二硝基苯合成路线 （共 755 条）
反应条件
potassium fluoride T=155°C;
参考文献
Finger; Kruse
Journal of the American Chemical Society, 1956 , vol. 78, p. 6034,6037
参考文献
Finger; Kruse
Journal of the American Chemical Society, 1956 , vol. 78, p. 6034,6037
反应条件
potassium hydroxide in ethanol
参考文献
Ilvespaeae,A.O.; Marxer,A.
Helvetica Chimica Acta, 1963 , vol. 46, p. 2009 - 2020
反应条件
ammonia; isopropylbenzene hydroperoxide in methanol; dichloromethane
参考文献
The Dow Chemical Company
Patent: US5414130 A1, 1995 ;
反应条件
sodium hydroxide; sodium hypophosphite; alpha,alpha-dimethylbenzyl hydroperoxide 1.) CH2Cl2, liquid NH3, -33 deg C, 1 h, 2.) -10 deg C; room temperature, 4 h; Yield given. Multistep reaction;
参考文献
Pews, R. Garth; Lysrnko, Zenon; Vosejpka, Paul C.
Journal of Organic Chemistry, 1997 , vol. 62, # 23 p. 8255 - 8256
反应条件
1.1: water; methanol / 0 - 30 °C 2.1: sodium sulfide; sodium hydrogencarbonate / water; methanol / 25 - 80 °C 3.1: 35 - 40 °C 3.2: 80 - 85 °C 3.3: 25 - 30 °C 4.1: hydrogen / Raney nickel / methanol / 25 - 30 °C / 4654.46 - 5171.62 Torr 5.1: N-ethyl-N,N-diisopropylamine / water / 25 - 95 °C 6.1: thionyl chloride / dichloromethane / 25 - 60 °C 6.2: 55 - 60 °C View Scheme
反应条件
1: 95 percent / acetonitrile / 72 h / Heating 2: 86 percent / ethanol; H2O / 24 h / 20 °C View Scheme
参考文献
Kamogawa, Hiroyoshi; Sato, Shigeki
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 1 p. 321 - 323
反应条件
hydrogenchloride; ethanol; sodium hydrogencarbonate 1,Nα-bis-<2,4-dinitro-phenyl>-l-histidine;
参考文献
Abderhalden; Blumberg
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1910 , vol. 65, p. 321
反应条件
potassium fluoride; tetra-phenylphosphonium bromide; tetraphthaloyl chloride in sulfolane; toluene T=190°C; 6 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 63, # 7 p. 2010 - 2017
反应条件
potassium hydroxide in ethanol 2 h; Heating;
参考文献
Mahmoud, Abdalla M.; El-Ezbawy, Samia R.; Abdel-Wahab, Aboel-Magd A.; El-Sherief, Hassan A. H.
Gazzetta Chimica Italiana, 1982 , vol. 112, # 1/2 p. 55 - 56
