1-氯-2,4-二硝基苯合成路线 （共 755 条）
反应条件
potassium hydroxide; diethyl ether
参考文献
Bartolotti; Passerini
Ricerca Scientifica, 1955 , vol. 25, p. 1095,1098
反应条件
1: 78 percent / sodium hydrogen carbonate / ethanol / 2 h / Heating
2: 56 percent / piperidine / ethanol / 2 h / Heating
3: 97 percent / cc. HCl / 4 h
4: 83 percent / 5M sodium hydroxide
View Scheme
参考文献
Harvey, Ian W.; McFarlane, Michael D.; Moody, David J.; Smith, David M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 681 - 690
参考文献
Cogolli,P. et al.
Journal of Organic Chemistry, 1979 , vol. 44, # 15 p. 2636 - 2642
反应条件
1: 91 percent / NaH / tetrahydrofuran / 24 h / 20 °C
2: CHCl3 / 24 h / 20 °C
View Scheme
参考文献
Nishiwaki, Nagatoshi; Nishida, Daisei; Ohnishi, Tetsuya; Hidaka, Fumie; Shimizu, Satoru; Tamura, Mina; Hori, Kazushige; Tohda, Yasuo; Ariga, Masahiro
Journal of Organic Chemistry, 2003 , vol. 68, # 22 p. 8650 - 8656
参考文献
Plucinski
Roczniki Chemii, 1959 , vol. 33, p. 1219
Chem.Abstr., 1960 , p. 10909
反应条件
ethanol; sodium acetate
参考文献
Sachs
Justus Liebigs Annalen der Chemie, 1909 , vol. 365, p. 162
参考文献
Roberts; Clark
Journal of the Chemical Society, 1935 , p. 1312
参考文献
Roberts; Clark
Journal of the Chemical Society, 1935 , p. 1312
反应条件
dibenzoyl peroxide in N,N-dimethyl-formamide
T=75°C; 10 h;
参考文献
Ivanova, T. M.; Shein, S. M.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 1055 - 1060
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 6 p. 1221 - 1228
反应条件
in ethanol; water
T=60°C; 6 h;
参考文献
Bil'kis, I. I.; Uskov, S. I.; Galdikov, V. S.; Shteingarts, V. D.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 6 p. 1123 - 1130
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 6 p. 1247 - 1255
