1-氯-2,4-二硝基苯合成路线 （共 755 条）
反应条件
ethanol; sodium hydrogencarbonate
参考文献
Leandri
Annali di Chimica (Rome, Italy), 1954 , vol. 44, p. 875,878
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydroxide in water; acetonitrile
T=20°C; Condensation; 8 h;
参考文献
Makosza; Voskresensky; Bialecki; Kwast
Polish Journal of Chemistry, 1999 , vol. 73, # 12 p. 1969 - 1977
参考文献
Giua; Marcellino; Curti
Gazzetta Chimica Italiana, 1920 , vol. 50 II, p. 302
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van der Kam
Recueil des Travaux Chimiques des Pays-Bas, 1926 , vol. 45, p. 732
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Ryan; Glover
Pr.irish Acad.<B>, 1917 , vol. 34, p. 102
反应条件
1: Et3N / ethanol / 4 h / Heating
2: 72 percent / hydrazine hydrate / Raney-Ni / ethanol; 1,2-dichloro-ethane / 3.5 h / 60 °C
3: 75 percent / tetrakis(acetonitrile)copper(I) tetrafluoroborate / toluene / 20 h / 80 - 90 °C
4: 95 percent / H2 / Raney-Ni / ethanol / 1 h / 760 Torr
View Scheme
参考文献
Knapp, Spencer; Ziv, Joseph; Rosen, Joseph D.
Tetrahedron, 1989 , vol. 45, # 5 p. 1293 - 1298
反应条件
2: tin dichloride; granulated tin; concentrated hydrochloric acid
View Scheme
参考文献
Kym
Chemische Berichte, 1899 , vol. 32, p. 3532
Chemische Berichte, 1900 , vol. 33, p. 449
反应条件
1: Cu / 200 °C
2: SnCl2, H2SO4
3: (i) NaNO2, AcOH, H2SO4, (ii) aq. H3PO2
View Scheme
参考文献
Forrest,J.
Journal of the Chemical Society, 1960 , p. 566 - 573
反应条件
ethanol; sodium ethanolate
参考文献
Nietzki; Schuendelen
Chemische Berichte, 1891 , vol. 24, p. 3588
参考文献
Nietzki; Schuendelen
Chemische Berichte, 1891 , vol. 24, p. 3588
反应条件
1: ethanol; aqueous NaOH-solution
2: sulfuric acid; nitric acid
View Scheme
参考文献
Clark
Industrial and Engineering Chemistry, 1933 , vol. 25, p. 1385
参考文献
Polaroid Corporation
Patent: US5262549 A1, 1993 ;
